Mestrelab Research S.L.v>%B$.AppleSystemUIFont@22{index}?$$.AppleSystemUIFont@22{name, 0}?nMestReNova14.0.0-23239zHXK{e~ e-  MestReNovaZ macOS 10.16dyn3155-240.wlan.ic.ac.ukL Delete Pagec49{J5[joshuadavies%\]ad-  MestReNovaZ macOS 10.16dyn3157-38.wlan.ic.ac.ukCreate Item (Text);r4%AѡX~<;joshuadavies%~A Text Item TypeTextt Type Report SpecialSubType Peaks,13CMetadatad-  MestReNovaZ macOS 10.16dyn3157-38.wlan.ic.ac.ukMove selection;r4%AѡX~<;joshuadavies% Text Item TypeText @ x5321 @ y6091d-  MestReNovaZ macOS 10.16dyn3157-38.wlan.ic.ac.ukEdit text item;r4%AѡX~<;joshuadavies%  Peak Report

13C NMR (101 MHz, CDCl3) δ 172.38, 171.64, 137.06, 136.61, 136.20, 129.67, 128.87, 128.76, 128.46, 128.21, 127.56, 127.03, 126.82, 55.20, 50.81, 37.05, 33.21.

Text Peak Report

13C NMR (101 MHz, CDCl3) δ 172.38, 171.64, 137.06, 136.61, 136.20, 129.67, 128.87, 128.76, 128.46, 128.21, 127.56, 127.03, 126.82, 55.20, 50.81, 37.05, 33.21.

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T/Volumes/Av400A/brad/nmr/Sep20-2021/50/fidData File Name =brukerExpName(datafile(_FILEPATH_), parm.txt(NAME), parm.txt(EXPNO), parm.txt(PROCNO))"Sep20-2021.50.fid Title *=Str.trimStr(title())jd-04-291 hComment  acqus ORIGIN&Bruker BioSpin GmbH Origin  acqus OWNERnmr Owner Site  acqus$INSTRUM spectInstrument  Author  acqus$SOLVENT CDCl3Solvent  acqus$TE293.9548Temperature  acqus$PULPROGzg30Pulse Sequence L=brukerExperimentType(acqus($PULPROG))1DExperiment  acqus$PROBHDT5 mm PABBO BB/19F-1H/D Z-GRD Z108618/0624 Probe  acqus$NS16Number of Scans  acqus$RG 111.61Receiver Gain  acqus $D[1]1 Relaxation Delay  acqus $P[1] 11.25Pulse Width  =brukerPresatFreq(acqus($PULPROG), acqus($SPOFFS[6]), acqus($SFO1), acqus($O1), acqus($SW), procs($OFFSET), fq0list()) .Presaturation Frequency j=brukerAQ(parm.txt(AQ;;;1), acqus($SW_h), acqus($TD))2.0447233 Acquisition Time v=brukerDate2(acqus($DATE), parm.txt(Date_), parm.txt(Time))&2021-09-20T11:26:00 Acquisition Date  acqus_LASTMODIFIED_&2021-09-20T11:26:42"Modification Date  Class   %100 Purity  0 Spectrum Quality 400.41240246,Spectrometer Frequency  8012.82051282051Spectral Width "-1603.95025642547 Lowest Frequency 1HNucleus .=Utl.div(acqus($TD), 2) 16384Acquired Size  65536Spectral Size  "0.122265938000801 $Digital Resolution $Absolute Reference. uxnmr.par%Vt8%VsҨ%Vv X`x\Ys6~&ڵRR(q#J IٞyIic O[!ՙz#_¡mM+OU^;L̍-i5K Ӂeږm[-ocd}W nyfX"x݊\.+ZQzs!DFLy~e¤uq}w d8` c"cpQ-Q8UDԇrl)hafº(M&Zẅ́7Qmϟ_YMJ~N2aJK%J<:O rt@X;Di퐣cCvHRCյJ4u{lh{lzDi(a2>ʵ:0}}=2iK{XڣȮ'B"I Ud"YzE6*rjPJ˘ #iyQH48H&>ZQQ#*r1dQ-ãxǻL֏?UaJTXwWO޾T= YH9/a\.X'Ԡz2(,zĊ>ir+jZnVRJ%eؠTjRkBjMH 7!&ф7! 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=L_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?ᙙ@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333       l_Z% a\?{B-?֧h|(% ?{B-?֧h|(?{B-?֧h|(@_oa\% _Z% _Z% _Z% _Z%   ?Ee0  !de0  !de0  !de0  !de0  !de0  !de0  !d? ? ? ? ? ? ? ?r b?:2ޗB,:?(:>. &֕?6C-@I???@& ?6C-?@$@$?@.@.@$ *@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{( 1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard(N/Ř$&@0zػԱ+@ecu@jue?F'B?F'B1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardvhQN9@0zػԱ+@b cL@.~?t??t?1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardbeD_\DC@0zػԱ+@RT<@8 b?t9M?t9M1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard^ B12C@@0zػԱ+@ʈ@):?r?._H?5?._H?51,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard+!]B btmT@0zػԱ+@^?x@EL??1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standardv,I_zVCT@0zػԱ+@N:'@~.S?3&U?3&U1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardF^rOG(c c@0zػԱ+@)M@%h?oTa?oTa1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardԆzqJӗT@0zػԱ+@ր`K@\? \1? \11,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard 53MeX[oMD@0zػԱ+@/49۫@ ?N=?N=1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard(bX@JEiǬO%@0zػԱ+@/VOM=@X6{?H̗uG?H̗uG1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardxW 4ETGף*b@0zػԱ+@J@ ??)a P5??)a P51,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardĀkOT5<@0zػԱ+@&skG@jB/K?<5?<5 T/Volumes/Av400A/brad/nmr/Sep20-2021/50/fide-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localx Create Page EF?ӂ@Zjoshuadavies%  At25e-  MestReNovaZ macOS 10.16dyn3155-240.wlan.ic.ac.ukv Paste PageBF^lF p#cjoshuadavies%\3  At2(66@'>|@r66 (#BF^lF p#cG?7m[ (@o0JK(!((''''''e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localFImport Item (NMR Spectrum)TؒH9C}< e}joshuadavies% r$ NMR Spectrum Item Type NMR Spectrum Filename V/Volumes/Av400A/brad/nmr/Dec07-2021/111/fidMetadatae-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localr ProcessingTؒH9C}< e}joshuadavies%!6 PCf1zeron oiDg8 first@QnCz Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321@ Parameterse-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localIncrease IntensityTؒH9C}< e}joshuadavies%9+ [-59.5091, 540.857] Scale[-59.5091, 540.857]e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.local Full Zoom OutTؒH9C}< e}joshuadavies%>t* [-20.7027, 240.67]$ Horizontal[-20.7027, 240.67]+ [-59.5091, 540.857]#Vertical[-59.5091, 540.857]e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localZoomTؒH9C}< e}joshuadavies%V+ [-10.3742, 190.593]% Horizontal[-10.3742, 190.593]+ [-59.5091, 540.857]#Vertical[-59.5091, 540.857]e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localDecrease IntensityTؒH9C}< e}joshuadavies%Z+ [-67.9065, 617.178] Scale[-67.9065, 617.178]e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localManual Peak PickingTؒH9C}< e}joshuadavies%f-D To@dO0From@fM!Region @8J# Threshold24.999256788211824 "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method StandardParamse-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localManual Peak PickingTؒH9C}< e}joshuadavies%lD To@\b From@ae Region @At4V" Threshold35.27698377802335 "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method StandardParamse-  MestReNovaZ macOS 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# # # # #               h: ! ) ! ) @4@(=# <????zG{??????????bD0$?@Y?zG{h: !  !  @4@( =# <?ٙC@@U???????h: ! ) ! ) @4@( =# =L_!@???ffffff?@V??ffffff?????????333333_!@???ffffff@@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333       l_Z% a\D+)P?`% D+)P?`.G0?aAw#a@`5\ a\% _Z% _Z% _Z% _Z%   ?Ee0  !de0 4P@nlC !de0  !de0  !de0  !de0  !de0  !d? ? ? ? ? ? ? ?r b?:2ޗB,:?(:>. &֕?6C-@I???@& ?6C-?@$@$?@.@.@$ *@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{* r SJB";@ h: !  !  @4@( =# <?ٙ-? ?@?@?d??zG{6,vq[VJ @r@@UnknownCDzd@ (\)@ =p @M@N?tzG{(@YAׄ@9%u*DSS methyl signal D2O@Y@Y@Y@Y@Yr b?:28,:?(:>. &֕?6C-@I???@& ?6C-?@@$?@.@.@$ & ?6C-??@Y?d 2D$????zG{8# # # # # # #               h: ! ) ! ) @4@(=# <????zG{??????????bD0$?@Y?zG{h: !  !  @4@( =# <?ٙC@@U???????h: ! ) ! ) @4@( =# =L_!@???ffffff?@V??ffffff?????????333333_!@???ffffff@@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333       l_Z% a\D+)P?`% D+)P?`.G0?aAw#a@`5\ a\% _Z% _Z% _Z% _Z%   ?Ee0  !de0 4P@nlC !de0  !de0  !de0  !de0  !de0  !d? ? ? ? ? ? ? ?r b?:2ޗB,:?(:>. &֕?6C-@I???@& ?6C-?@$@$?@.@.@$ *@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{+I(1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardCJu\t@nlu4т@eGC@BSu?@?@1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard ^@@Fl@nlu4т@et|U@A㜄e?zE /?zE /1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardIuHj @nlu4т@a!H[@LJQίd?v%?v%1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard@þmE,_ @nlu4т@a{@u@Idx(? 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Iq1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardypI8o@nlu4т@aFK@Pw2?)!=o?)!=o1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardĂ6?F+M@nlu4т@`5N?t|>1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard?4L#BɞWXH@nlu4т@`I v@s\C=?!?!1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard>,|eIt|@nlu4т@`ke!@trM,?\w?\w1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard\t}HK$ݱf0@nlu4т@`N@{[hk?b?b1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard#Q]{@ D @nlu4т@`I@og??1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard |GҺv)@nlu4т@_ ̢@j!.r8_?|˻>?|˻>1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard%IP'J_׹>@nlu4т@_J0E@rY6??1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardorElMSݾ@nlu4т@_/ꎞ@wJ>G?1@?1@1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard'ZCC0nL@nlu4т@Kp}3_@`-0*?('