1-cyclopentyl-3-(2-isopropyl-5-methylphenoxy)propan-2-one

DOI: 10.14469/hpc/8126 Metadata

Created: 2021-04-26 09:04

Last modified: 2021-04-26 10:00

Author: Lu Qian

License: Creative Commons: Public Domain Dedication 1.0

Funding: (none given)

Description

0.749 g of thymol and 0.714 g of Cyclopentylacetic acid was measured out. In a round bottom flask with a magnetic stirrer bar, 15mL of acetonitrile, 0.5 mmol of DMAP and 6.5 mmol of EDC·HCl was added. Then the acid and thymol were added add with the aid of acetonitrile (10 mL) each. Heater and stirring was turned on after the condenser was set to run (100 °C). TLC assessments were carried out every hour to monitor the reaction process. At the end of the day, stopped the water running and heater block. The reaction solution appeared to be transparent at room temperature.

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FilenameSizeTypeDescription
1-cyclopentyl-3-(2-isopropyl-5-methylphenoxy)propan-2-one.zip 4MB application/zip zip file of original data
1-cyclopentyl-3-(2-isopropyl-5-methylphenoxy)propan-2-one.mnpub 0 chemical/x-mnpub Mestrenova signature file for 1-cyclopentyl-3-(2-isopropyl-5-methylphenoxy)propan-2-one.zip
1-cyclopentyl-3-(2-isopropyl-5-methylphenoxy)propan-2-one.svg 189KB image/svg+xml svg file
1-cyclopentyl-3-(2-isopropyl-5-methylphenoxy)propan-2-one.png 47KB image/png png file
1-cyclopentyl-3-(2-isopropyl-5-methylphenoxy)propan-2-one.nmrium 4MB application/octet-stream NMRium file
1-cyclopentyl-3-(2-isopropyl-5-methylphenoxy)propan-2-one.cdxml 6KB chemical/x-cdxml chemdraw file

Member of collection / collaboration

DOIDescription
10.14469/hpc/6215 1st Year undergraduate synthesis 1.2 laboratory (2019-2020)

Subject Keywords

KeywordValue
inchi InChI=1S/C18H26O2/c1-13(2)17-9-8-14(3)10-16(17)12-20-18(19)11-15-6-4-5-7-15/h8-10,13,15H,4-7,11-12H2,1-3H3
inchikey JDDJBCCDXDPQCH-UHFFFAOYSA-N

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