4-allyl-2-methoxyphenyl cyclohexanecarboxylate
DOI: 10.14469/hpc/7155 Metadata
Created: 2020-04-29 13:35
Last modified: 2020-05-01 05:35
License: Creative Commons: Public Domain Dedication 1.0
Funding: (none given)
Description
A 15 mL acetonitrile solution was mixed with DMAP (0.0064 g, 0.5 mmol) and EDC.HCl (1.25 g, 6.5 mmol) and refluxed at 92 oC with Cyclohexanecarboxylic acid (0.788 g, 6.15 mmol) and Eugenol (0.826 g, 5.03 mmol). It was cooled at room temperature for a day and a work-up was done to extract the organic layer (Ester & Hexane) which was purified under a rotary evaporator (at 40 oC) to produce the crystallised ester (0.78 g, 2.85 mmol, 56.5% yield).
Files
| Filename | Size | Type | Description |
|---|---|---|---|
| NMR data.zip | 454KB | application/zip | Ester NMR data |
| NMR data.mnpub | 0 | chemical/x-mnpub | Mestrenova signature file for NMR data.zip |
| Chemdraw Data.cdxml | 10KB | chemical/x-cdxml | Ester Chemdraw file |
Member of collection / collaboration
| DOI | Description |
|---|---|
| 10.14469/hpc/6215 | 1st Year undergraduate synthesis 1.2 laboratory (2019-2020) |
Subject Keywords
| Keyword | Value |
|---|---|
| inchi | InChI=1S/C17H22O3/c1-3-7-13-10-11-15(16(12-13)19-2)20-17(18)14-8-5-4-6-9-14/h3,10-12,14H,1,4-9H2,2H3 |
| inchikey | CKKDRUZRAKGJDP-UHFFFAOYSA-N |