4-allyl-2-methoxyphenyl 4-(triflouromethyl)cyclohexane-1-carboxylate
DOI: 10.14469/hpc/7126 Metadata
Created: 2020-04-22 20:25
Last modified: 2020-04-24 09:25
License: Creative Commons: Public Domain Dedication 1.0
Funding: (none given)
Description
The phenol eugenol (0.86 g) was refluxed at 82 oC with 4-trifluoromethylcyclohexanecarboxylic acid (1.0350 g) in the presence of EDC.HCl (1.25 g, 6.5 mmol) and DMAP (0.0064 g, 0.5 mmol) as a catalyst with 30 mL acetonitrile as a solvent to form the ester 4-allyl-2-methoxyphenyl 4-(triflouromethyl)cyclohexane-1-carboxylate. The remaining hexane was removed through rotary evaporation at 40 oC to leave a colourless liquid (0.546 g, 32.96%) which solidified when brought to room temperature. The IR and proton NMR spectra were recorded.
Files
| Filename | Size | Type | Description |
|---|---|---|---|
| 4-allyl-2-methoxyphenyl 4-(triflouromethyl)cyclohexane-1-carboxylate.cdxml | 7KB | chemical/x-cdxml | ChemDraw description of module |
| 4-allyl-2-methoxyphenyl 4-(triflouromethyl)cyclohexane-1-carboxylate.mnova | 294KB | chemical/x-mnova | MestReNova Dataset |
| 4-allyl-2-methoxyphenyl 4-(triflouromethyl)cyclohexane-1-carboxylate.mnpub | 0 | chemical/x-mnpub | Mestrenova signature file for 4-allyl-2-methoxyphenyl 4-(triflouromethyl)cyclohexane-1-carboxylate.mnova |
| 4-allyl-2-methoxyphenyl 4-(trifluoromethyl)cyclohexane-1-carboxylate.zip | 451KB | application/zip | Raw data |
| 4-allyl-2-methoxyphenyl 4-(trifluoromethyl)cyclohexane-1-carboxylate.mnpub | 0 | chemical/x-mnpub | Mestrenova signature file for 4-allyl-2-methoxyphenyl 4-(trifluoromethyl)cyclohexane-1-carboxylate.zip |
Member of collection / collaboration
| DOI | Description |
|---|---|
| 10.14469/hpc/6215 | 1st Year undergraduate synthesis 1.2 laboratory (2019-2020) |
Subject Keywords
| Keyword | Value |
|---|---|
| inchi | InChI=1S/C18H21F3O3/c1-3-4-12-5-10-15(16(11-12)23-2)24-17(22)13-6-8-14(9-7-13)18(19,20)21/h3,5,10-11,13-14H,1,4,6-9H2,2H3 |
| inchikey | IJNBTIZKLBFNES-UHFFFAOYSA-N |