DOI: 10.14469/hpc/6885 Metadata

Created: 2020-02-28 11:48

Last modified: 2020-02-28 15:16

Author: Marzuq Khan

License: Creative Commons: Public Domain Dedication 1.0

Funding: (none given)

Description

Non-purified esterification of 5 mmol of guaiacol and 5.5 mmol behenic acid. Reaction mixture of starting materials along with DMAP and EDC.HCL in acetonitrile refluxed at 90 degrees Celsius for an hour. Washed mixture using hydrochloric acid then sodium bicarbonate then water then brine. Dried with magnesium sulfate and filtered under gravity. Used rotary evaporator to remove solvent.

Files

Filename	Size	Type	Description
NMR.mnova	211KB	chemical/x-mnova	MestReNova file
NMR.mnpub	0	chemical/x-mnpub	Mestrenova signature file for NMR.mnova
NMR.jcamp	408KB	application/octet-stream	JCAMP file
550.zip	447KB	application/zip	Bruker data
550.mnpub	0	chemical/x-mnpub	Mestrenova signature file for 550.zip
Ester.cdxml	7KB	chemical/x-cdxml	Structure

Member of collection / collaboration

DOI	Description
10.14469/hpc/6215	1st Year undergraduate synthesis 1.2 laboratory (2019-2020)

Subject Keywords

Keyword	Value
inchi	InChI=1S/C29H50O3/c1-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-26-29(30)32-28-25-23-22-24-27(28)31-2/h22-25H,3-21,26H2,1-2H3
inchikey	BDSLEOKQUPUXSO-UHFFFAOYSA-N

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