User-Friendly Copper-Catalysed Reduction of Azides to Amines

DOI: 10.14469/hpc/6099 Metadata

Created: 2019-09-16 11:42

Last modified: 2024-11-27 17:05

Author: Silvia Diez-Gonzalez

License: Creative Commons: Public Domain Dedication 1.0

Funding: (none given)

Co-author: Andrew White

Description

Three homoleptic copper(I) complexes have been prepared and applied to the reduction of organic azides. Under optimised conditions, complex [Cu(HPDIDMA)2]BF4 3 (HPDIDMA = 2,6-bis[N-(4-dimethylaminophenyl)carbaldimino]pyridine) could reduce a range of electron-poor azides in a mixture of DMSO and water without the need of an additional H-source.

Members

DOIDescription
10.14469/hpc/6100 Cu-PDI reduction of azides - NMR Data
10.14469/hpc/6101 Cu-PDI reduction of azides - Crystallographic Data

Associated DOIs

Current dataset ...DOIDescription
References 10.1002/ajoc.201900555 Published reference

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