Acid-Mediated Ring-Expansion of 2,2-Disubstituted Azetidine Carbamates to 6,6 Disubstituted 1,3-Oxazinan-2-ones
DOI: 10.14469/hpc/4982 Metadata
Created: 2019-01-29 17:11
Last modified: 2019-04-02 17:19
License: Creative Commons: Public Domain Dedication 1.0
Funding: (none given)
Co-author: Alan Spivey Co-author: James A. Bull Co-author: Christopher Cordier
Description
Characterisation data for compounds from "Acid-Mediated Ring-Expansion of 2,2-Disubstituted Azetidine Car-bamates to 6,6 Disubstituted 1,3-Oxazinan-2-ones"
Files
| Filename | Size | Type | Description |
|---|---|---|---|
| 1. Diazo Compounds (8n and 8o).zip | 2MB | application/zip | Data for Diazo Compounds 8n and 8o (raw NMR data, mnova file for processed data, IR and HRMS) |
| 1. Diazo Compounds (8n and 8o).mnpub | 0 | chemical/x-mnpub | Mestrenova signature file for 1. Diazo Compounds (8n and 8o).zip |
| 2. Azetidine Carbamates (9j,l,m).zip | 6MB | application/zip | Data for Azetidine Carbamates 9j,l and m (raw NMR data, mnova file for processed data, IR and HRMS) |
| 2. Azetidine Carbamates (9j,l,m).mnpub | 0 | chemical/x-mnpub | Mestrenova signature file for 2. Azetidine Carbamates (9j,l,m).zip |
| 3. Oxazinanones by 4- to 6-Ring Expansion (2, 4a–j,l).zip | 34MB | application/zip | Data for Oxazinanones 2, 4a to j and 4l (raw NMR data, mnova file for processed data, IR and HRMS) |
| 3. Oxazinanones by 4- to 6-Ring Expansion (2, 4a–j,l).mnpub | 0 | chemical/x-mnpub | Mestrenova signature file for 3. Oxazinanones by 4- to 6-Ring Expansion (2, 4a–j,l).zip |
| 4. Deprotected Azetidines and Pyrrolidines (5a,j,k and 11).zip | 5MB | application/zip | Data for Deprotected Azetidines and Pyrrolidines 5a,j,k and 11 (raw NMR data, mnova file for processed data, IR and HRMS) |
| 4. Deprotected Azetidines and Pyrrolidines (5a,j,k and 11).mnpub | 0 | chemical/x-mnpub | Mestrenova signature file for 4. Deprotected Azetidines and Pyrrolidines (5a,j,k and 11).zip |
| 5. Oxazinanones by NICE Reaction (4k,n–p).zip | 6MB | application/zip | Data for Oxazinanones 4k and 4n to 4p (raw NMR data, mnova file for processed data, IR and HRMS) |
| 5. Oxazinanones by NICE Reaction (4k,n–p).mnpub | 0 | chemical/x-mnpub | Mestrenova signature file for 5. Oxazinanones by NICE Reaction (4k,n–p).zip |
| 6. Functionalization of oxazinanones (13–17).zip | 26MB | application/zip | Data for Oxazinanones 13to 17 (raw NMR data, mnova file for processed data, IR and HRMS) |
| 6. Functionalization of oxazinanones (13–17).mnpub | 0 | chemical/x-mnpub | Mestrenova signature file for 6. Functionalization of oxazinanones (13–17).zip |
Associated DOIs
| Current dataset ... | DOI | Description |
|---|---|---|
| References | 10.1021/acs.orglett.9b00407 | doi for paper titled "Acid-Mediated Ring Expansion of 2,2-Disubstituted Azetidine Carbamates to 6,6-Disubstituted 1,3-Oxazinan-2-ones" published in Organic Letters |