NMR Data for compound 38c. 2-chlorophenylboronic acid + 2-aminopyridine

DOI: 10.14469/hpc/14847 Metadata

Created: 2024-11-09 14:01

Last modified: 2025-02-09 16:59

Author: Henry Rzepa

License: Creative Commons: Public Domain Dedication 1.0

Funding: (none given)

Description

Under an atmosphere of argon, 2-chlorophenyl boronic acid (47 mg, 0.3 mmol, 3 eq.) and 2-aminopyridine (10 mg, 0.1 mmol, 1 eq.) were suspended in CDCl3 (1.2 ml), and activated 4Å molecular sieves (1.2 g) were added. The reaction was stirred for 3 days, after which time it was filtered and 1H and 11B NMR spectra were measured, revealing a product identical to that obtained using the pre-formed boroxine

Member of collection / collaboration

DOIDescription
10.14469/hpc/14846 NMR Data for compound 38. Boroxine and boronic acid - amine complexes

Members

DOIDescription
10.14469/hpc/14868 NMR Data for 38c. 2-chlorophenylboronic acid + 2-aminopyridine. 1H
10.14469/hpc/14869 NMR Data for 38c. 2-chlorophenylboronic acid + 2-aminopyridine. 11B

Subject Keywords

KeywordValue
Inchi InChI=1S/C22H20B3Cl3N2O3/c1-3-17(16(2)26)23-31-24(18-10-4-6-12-20(18)27)33-25(32-23,19-11-5-7-13-21(19)28)30-15-9-8-14-22(30)29/h3-15H,2,29H2,1H3/b17-3+
Inchikey XVERRFABOLUYPR-IJUHEHPCSA-N

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