NMR data for compound 31. N-(pyridin-2-yl)-2-(thiophen-3-yl)acetamide

DOI: 10.14469/hpc/14740 Metadata

Created: 2024-11-02 07:00

Last modified: 2025-02-08 14:20

Author: Henry Rzepa

License: Creative Commons: Public Domain Dedication 1.0

Funding: (none given)

Description

Synthesised according to the general procedure. Purified by flash column chromatography. Yield = 866 mg, off white solid, 79%. Data is in accordance with previous reports.19 1H NMR (700 MHz, CDCl3) δ (ppm) = 8.27 (s, 1H), 8.22 (m, 2H), 7.69 (ddd, J = 8.4 ,7.5, 1.9 Hz, 1H), 7.36 (dd, J = 4.9, 3.0 Hz, 1H), 7.20 (m, 1H), 7.06 (dd, J = 4.9, 1.3 Hz, 1H), 7.02 (ddd, J = 7.4, 4.9, 0.9 Hz, 1H), 3.78 (s, 2H). 13C NMR (176 MHz, CDCl3) δ (ppm) = 169.3, 151.4, 147.9, 138.6, 133.9, 128.5, 127.2, 124.0, 120.1, 114.2, 39.4. HRMS [C11H10N2OS+H]+ ; expected : 219.0587, observed : 219.0585 Melting point: 108 – 109 °C

Member of collection / collaboration

DOIDescription
10.14469/hpc/14635 Borate-Catalysed Direct Amidation Reactions of Coordinating Substrates. NMR data

Members

DOIDescription
10.14469/hpc/14805 NMR data for compound 31. N-(pyridin-2-yl)-2-(thiophen-3-yl)acetamide. 1H
10.14469/hpc/14806 NMR data for compound 31. N-(pyridin-2-yl)-2-(thiophen-3-yl)acetamide. 13C

Subject Keywords

KeywordValue
Inchi InChI=1S/C11H10N2OS/c14-11(7-9-4-6-15-8-9)13-10-3-1-2-5-12-10/h1-6,8H,7H2,(H,12,13,14)
Inchikey IGKQDUDWOGGVJL-UHFFFAOYSA-N

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