NMR data for compound 26. N-((3s,5s,7s)-adamantan-1-yl)-2-phenylacetamide

DOI: 10.14469/hpc/14736 Metadata

Created: 2024-11-01 17:02

Last modified: 2024-11-05 18:40

Author: Henry Rzepa

License: Creative Commons: Public Domain Dedication 1.0

Funding: (none given)

Description

Synthesised according to the general procedure. Purified by flash column chromatography (EtOAc 10% à 50% in cyclohexane) Yield = 67 mg white solid, 5%. Data is in accordance with previous literature values.17 1H NMR (700 MHz, CDCl3) δ (ppm) = 7.34 (t, J = 7.4 Hz, 1H), 7.27 (t, J = 7.4 Hz, 2H), 7.24 (d, J = 7.5 Hz, 2H), 5.02 (s, 1H), 3.47 (s, 2H), 2.00 – 2.05 (m, 3H), 1.88 – 1.92 (m, 6H), 1.64 (t, J = 3.0 Hz, 6H). 13C NMR (176 MHz, CDCl3) δ (ppm) = 170.2, 135.7, 129.4, 129.0, 127.2, 52.0, 45.2, 41.6, 36.4, 29.5. HRMS : [C18H23ON + H]+ : Expected = 270.1852, found 270.1855

Member of collection / collaboration

DOIDescription
10.14469/hpc/14635 Borate-Catalysed Direct Amidation Reactions of Coordinating Substrates. NMR data

Members

DOIDescription
10.14469/hpc/14798 NMR data for compound 26. N-((3s,5s,7s)-adamantan-1-yl)-2-phenylacetamide. 13C
10.14469/hpc/14797 NMR data for compound 26. N-((3s,5s,7s)-adamantan-1-yl)-2-phenylacetamide. 1H

Subject Keywords

KeywordValue
Inchi InChI=1S/C18H23NO/c20-17(9-13-4-2-1-3-5-13)19-18-10-14-6-15(11-18)8-16(7-14)12-18/h1-5,14-16H,6-12H2,(H,19,20)
Inchikey PILCMWJBOSRDPC-UHFFFAOYSA-N

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