NMR data for compound 25. N-cyclohexylcyclopropanecarboxamide

DOI: 10.14469/hpc/14735 Metadata

Created: 2024-11-01 17:00

Last modified: 2024-11-05 18:38

Author: Henry Rzepa

License: Creative Commons: Public Domain Dedication 1.0

Funding: (none given)

Description

Synthesised according to the general procedure. Purified by flash column chromatography (EtOAc : cyclohexane, 25% à 85%). Yield = 812 mg white solid, 97%. Data in accordance with previous literature reports.16 1H NMR (700 MHz, CDCl3): δ (ppm) = 5.54 (s, 1H), 3.77 (tdt, J = 12 Hz, 11 Hz, 4 Hz, 1H), 1.91 (dddd, J = 12.5 Hz, 4 Hz, 3.9 Hz, 3.5 Hz, 2H), 1.69 (dtt, J = 13.5, 3.9, 3.9 Hz, 2H), 1.60 (dtt, J = 12.0, 3.9, 3.9 Hz, 1 H), 1.34 (qt, J = 12.1 Hz, 3.5 Hz, 2H), 1.27 (tt, J = 7.9 Hz, 4.4 Hz, 1H), 1.08-1.18 (m, 3H), 0.93 (dtd, J = 4.4 Hz, 3.9 Hz, 3.1 Hz, 2H), 0.69 (dtd, J = 7.9 Hz, 3.9 Hz, 3.1 Hz, 2H). 13C NMR (176 MHz, CDCl3): δ (ppm) = 172.6, 48.4, 33.5, 25.7, 25.1, 15.0, 7.1 HRMS : [C10H17ON + H]+ : Expected = 168.1383, found 168.1388 Melting point : 137 – 138 °C

Member of collection / collaboration

DOIDescription
10.14469/hpc/14635 Borate-Catalysed Direct Amidation Reactions of Coordinating Substrates. NMR data

Members

DOIDescription
10.14469/hpc/14796 NMR data for compound 25. N-cyclohexylcyclopropanecarboxamide. 13C
10.14469/hpc/14795 NMR data for compound 25. N-cyclohexylcyclopropanecarboxamide. 1H

Subject Keywords

KeywordValue
Inchi InChI=1S/C10H17NO/c12-10(8-6-7-8)11-9-4-2-1-3-5-9/h8-9H,1-7H2,(H,11,12)
Inchikey SNRVHASXCDZNDP-UHFFFAOYSA-N

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