NMR data for compound 23. N-allyl-N,2-diphenylacetamide

DOI: 10.14469/hpc/14733 Metadata

Created: 2024-11-01 16:57

Last modified: 2024-11-05 18:37

Author: Henry Rzepa

License: Creative Commons: Public Domain Dedication 1.0

Funding: (none given)

Description

Synthesised according to the general procedure using toluene as reaction solvent for 23 hours. Purified by flash column chromatography (EtOAc 20% à 60% in cyclohexane) Yield = 440 mg brown oil, 42%. Analytical data is in accordance with reported literature values.15 1H NMR (700 MHz, CDCl3) δ (ppm) = 7.29 (d, J = 7.5 Hz, 2H), 7.24-7.20 (m, 3H), 7.16-7.12 (m, 3H), 7.03 (d, J = 7.9Hz, 2H), 3.50 (s, 3H). 13C NMR (176 MHz, CDCl3) δ (ppm) = 170.8, 145.0, 136.0, 129.7, 129.3, 128.8, 127.9, 127.0, 126.6, 38.5.

Member of collection / collaboration

DOIDescription
10.14469/hpc/14635 Borate-Catalysed Direct Amidation Reactions of Coordinating Substrates. NMR data

Members

DOIDescription
10.14469/hpc/14791 NMR data for compound 23. N-allyl-N,2-diphenylacetamide. 1H
10.14469/hpc/14792 NMR data for compound 23. N-allyl-N,2-diphenylacetamide. 13C

Subject Keywords

KeywordValue
inchi InChI=1S/C17H17NO/c1-2-13-18(16-11-7-4-8-12-16)17(19)14-15-9-5-3-6-10-15/h2-12H,1,13-14H2
Inchikey HJCBTDZWRKUNCG-UHFFFAOYSA-N

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