NMR data for compound 11. N-phenylpicolinamide

DOI: 10.14469/hpc/14717 Metadata

Created: 2024-11-01 15:21

Last modified: 2024-11-05 18:03

Author: Henry Rzepa

License: Creative Commons: Public Domain Dedication 1.0

Funding: (none given)

Description

Synthesised according to the general procedure. After aqueous work-up, the crude oil was triturated with pentane and dried under vacuum to yield an orange/brown crystalline solid. Yield = 427 mg, 43%. Analytical data is in accordance with literature reports.9 1H NMR (700 MHz, CDCl3) δ(ppm) = 10.04 (s, 1H), 8.61 (d, J = 4.1 Hz, 1H), 8.31 (d, J = 7.8 Hz, 1H), 7.91 (t, J = 7.6 Hz, 1H), 7.79 (d, J = 7.9 Hz, 2H), 7.48 (dd, J = 7.7, 5.1 Hz, 1H), 7.39 (t, J = 7.7 Hz, 2H), 7.15 (t, J = 7.4 Hz, 1H). 13C NMR (176 MHz, CDCl3) δ(ppm) = 162.1, 149.9, 148.0, 137.9, 137.9, 129.2, 126.6, 124.5, 122.6, 119.8. HRMS [C12H10N2O+H]+ : Expected 199.0866 Observed 199.0866 Melting point: 71 – 73 °C

Member of collection / collaboration

DOIDescription
10.14469/hpc/14635 Borate-Catalysed Direct Amidation Reactions of Coordinating Substrates. NMR data

Members

DOIDescription
10.14469/hpc/14763 NMR data for compound 11. N-phenylpicolinamide. 1H
10.14469/hpc/14764 NMR data for compound 11. N-phenylpicolinamide. 13C

Subject Keywords

KeywordValue
Inchi InChI=1S/C12H10N2O/c15-12(11-8-4-5-9-13-11)14-10-6-2-1-3-7-10/h1-9H,(H,14,15)
Inchikey GVBHRBMWXDCRHZ-UHFFFAOYSA-N

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