NMR data for compound 10. 2-phenyl-N-(1H-pyrazol-3-yl)acetamide

DOI: 10.14469/hpc/14716 Metadata

Created: 2024-11-01 15:20

Last modified: 2024-11-05 17:58

Author: Henry Rzepa

License: Creative Commons: Public Domain Dedication 1.0

Funding: (none given)

Description

Synthesised according to the general procedure. Purified by recrystallisation from hot methanol/water (2:1, 21 ml). Yield = 753 mg white needle crystals, 3.75 mmol, 75%. Analytical data is in accordance with literature reports.8 1H NMR (700 MHz, DMSO) δ(ppm) = 12.30 (s, 1H), 10.59 (s, 1H), 7.56 (s, 1H), 7.30 (m, 4H), 7.22 (t, J = 6.7 Hz, 1H), 6.46 (s, 1H), 3.59 (s, 2H). 13C NMR (176 MHz, DMSO) δ(ppm) = 168.2, 147.4, 136.2, 129.1, 128.6, 128.3, 126.5, 95.9, 42.5. HRMS [C11H11N3O+H]+ : Expected 202.0975 Observed 202.0971 Melting point: 150 – 152 °C

Member of collection / collaboration

DOIDescription
10.14469/hpc/14635 Borate-Catalysed Direct Amidation Reactions of Coordinating Substrates. NMR data

Members

DOIDescription
10.14469/hpc/14762 NMR data for compound 10. 2-phenyl-N-(1H-pyrazol-3-yl)acetamide. 13C
10.14469/hpc/14761 NMR data for compound 10. 2-phenyl-N-(1H-pyrazol-3-yl)acetamide. 1H

Subject Keywords

KeywordValue
Inchi InChI=1S/C11H11N3O/c15-11(13-10-6-7-12-14-10)8-9-4-2-1-3-5-9/h1-7H,8H2,(H2,12,13,14,15)
Inchikey PVSBXANMTPUBOW-UHFFFAOYSA-N

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