NMR data for compound 9. N-(2-(dimethylamino)ethyl)-2-phenylacetamide

DOI: 10.14469/hpc/14715 Metadata

Created: 2024-11-01 15:19

Last modified: 2024-11-05 17:57

Author: Henry Rzepa

License: Creative Commons: Public Domain Dedication 1.0

Funding: (none given)

Description

Synthesised according to the general procedure. Purified by flash column chromatography (MeOH in DCM, 5 à 25 %, plus 1% NEt3). Yield = 926 mg cream coloured hygroscopic solid, 4.49 mmol, 90%. 1H NMR (600 MHz, CDCl3) δ (ppm) = 7.33 (m, 2H), 7.27 (m, 3 H), 6.03 (s, 1H), 3.55 (s, 2H), 3.28 (q, J = 5.8 Hz, 2H), 2.33 (t, J = 6.0 Hz, 2H), 2.15 (s, 6 H). 13C NMR (151 MHz, CDCl3) δ (ppm) = 171.1, 135.2, 129.4, 128.9, 127.2, 57.5, 45.2, 43.8, 37.1. HRMS [C12H18N2O + H]+ ; Calculated 207.1492, observed 207.1488 νmax (solid/cm-1): 3921, 3080, 3060, 3027, 2982, 2976, 2941, 2815, 2761, 1636, 1550, 1493, 1466, 1452, 1446

Member of collection / collaboration

DOIDescription
10.14469/hpc/14635 Borate-Catalysed Direct Amidation Reactions of Coordinating Substrates. NMR data

Members

DOIDescription
10.14469/hpc/14759 NMR data for compound 9. N-(2-(dimethylamino)ethyl)-2-phenylacetamide. 1H
10.14469/hpc/14760 NMR data for compound 9. N-(2-(dimethylamino)ethyl)-2-phenylacetamide. 13C

Subject Keywords

KeywordValue
Inchi InChI=1S/C12H18N2O/c1-14(2)9-8-13-12(15)10-11-6-4-3-5-7-11/h3-7H,8-10H2,1-2H3,(H,13,15)
Inchikey SKGYVELDSNNACR-UHFFFAOYSA-N

Edit