NMR data for compound 6. 2-phenyl-N-(quinolin-8-yl)acetamide

DOI: 10.14469/hpc/14712 Metadata

Created: 2024-11-01 15:15

Last modified: 2024-11-05 17:52

Author: Henry Rzepa

License: Creative Commons: Public Domain Dedication 1.0

Funding: (none given)

Description

Synthesised according to the general procedure. Purified by flash column chromatography (EtOAc : Cyclohexane 10% à 30%). Yield = 1.16g off-white solid, 4.42 mmol, 88%. Analytical data is in accordance with literature reports.6 1H NMR (700 MHz, CDCl3) δ (ppm) = 9.92 (s, 1H), 8.76 (d, J = 7.5 Hz, 1H), 8.69 (dd, J = 4.2, 1.5 Hz, 1H), 8.11 (dd, J = 8.2, 1.4 Hz, 1H), 7.51 (t, J = 7.9 Hz, 1H), 7.47 (dd, J = 8.1, 1 Hz, 1H), 7.45 (d, J = 7.5 Hz, 2H), 7.40 (m, 3H), 7.33 (t, J = 7.3 Hz, 1H), 3.90 (s, 2H). 13C NMR (176 MHz, CDCl3) δ (ppm) = 169.7, 148.2, 138.5, 136.5, 134.8, 134.59, 129.7, 129.1, 128.0, 127.5, 127.5, 121.75, 121.7, 116.6, 45.5 HRMS [C17H14N2O+H]+ : Expected 263.1179, Observed 263.1178 Melting point : 71 - 73 °C

Member of collection / collaboration

DOIDescription
10.14469/hpc/14635 Borate-Catalysed Direct Amidation Reactions of Coordinating Substrates. NMR data

Members

DOIDescription
10.14469/hpc/14754 NMR data for compound 6. 2-phenyl-N-(quinolin-8-yl)acetamide. 13C
10.14469/hpc/14753 NMR data for compound 6. 2-phenyl-N-(quinolin-8-yl)acetamide. 1H

Subject Keywords

KeywordValue
Inchi nChI=1S/C17H14N2O/c20-16(12-13-6-2-1-3-7-13)19-15-10-4-8-14-9-5-11-18-17(14)15/h1-11H,12H2,(H,19,20)
Inchikey FDOZLJKPVDSIBO-UHFFFAOYSA-N

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