(Rax)-4-(((1R,2R)-2-Bromocyclohexyl)oxy)-2,6-di(phenanthren-9-yl)dinaphtho[2,1-d1',2'-f][1,3,2]dioxaphosphepine 4-oxide (4.6)

DOI: 10.14469/hpc/14482 Metadata

Created: 2024-07-24 15:31

Last modified: 2024-08-01 14:16

Author: Ben Lancaster

License: Creative Commons: Attribution 4.0

Funding: (none given)

Description

NMR, IR, HRMS, HPLC, and X-ray data for (Rax)-4-(((1R,2R)-2-bromocyclohexyl)oxy)-2,6-di(phenanthren-9-yl)dinaphtho[2,1-d1',2'-f][1,3,2]dioxaphosphepine 4-oxide (4.6)

Files

FilenameSizeTypeDescription
NMR Spectra.mnova 1MB chemical/x-mnova NMR Spectrum
NMR Spectra.mnpub 0 chemical/x-mnpub Mestrenova signature file for NMR Spectra.mnova
IR Spectrum.a2r 32KB application/octet-stream IR Spectrum
HPLC (Rax,1R,2R)-Diastereomer.pdf 35KB application/pdf HPLC (Rax,1R,2R)-Diastereomer
HPLC (Rax,1R,2R)-Diastereomer Report.pdf 11KB application/pdf HPLC (Rax,1R,2R)-Diastereomer Report
HPLC (Rax,1S,2S)-Diastereomer.pdf 34KB application/pdf HPLC (Rax,1S,2S)-Diastereomer
HPLC (Rax,1S,2S)-Diastereomer Report.pdf 11KB application/pdf HPLC (Rax,1S,2S)-Diastereomer Report
Mass Spectrum.pdf 140KB application/pdf Mass Spectrum
HPLC Mixture.pdf 35KB application/pdf HPLC Mixture (56:44 dr)
HPLC Mixture Report.pdf 12KB application/pdf HPLC Mixture (56:44 dr) Report
CB2303.doc 34KB application/msword Crystal Data and Structure Refinement
CB2303_x.cif 23KB chemical/x-cif CIF File
CB2303-PL1.png 405KB image/png X-Ray Structure

Member of collection / collaboration

DOIDescription
10.14469/hpc/14446 Chapter 4

Subject Keywords

KeywordValue
inchi InChI=1S/C47H29BrO4P.2C3H3.CH2.H/c1-5-43(30(4)48)50-53(49)51-46-39(41-26-33-16-8-10-18-35(33)37-20-12-13-21-38(37)41)23-22-28(2)44(46)45-36-19-11-9-17-34(36)27-42(47(45)52-53)40-25-32-15-7-6-14-31(32)24-29(40)3;2*1-3-2;;/h2-4,6-21,23,25-27,30,43H,1,5H2;2*1-3H;1H2;/t30-,43-,53-;;;;/m1..../s1
inchikey RPDSMAALVRAMQK-KBCHEFSFSA-N

Edit