rac-3,3'-Di(phenanthren-9-yl)-[1,1'-binaphthalene]-2,2'-diyl phosphorochloridate (rac-6)
DOI: 10.14469/hpc/14353 Metadata
Created: 2024-06-18 14:18
Last modified: 2024-07-05 15:04
License: Creative Commons: Public Domain Dedication 1.0
Funding: (none given)
Description
NMR, IR, HRMS, and HPLC data for rac-3,3'-di(phenanthren-9-yl)-[1,1'-binaphthalene]-2,2'-diyl phosphorochloridate (rac-6)
Files
Filename | Size | Type | Description |
---|---|---|---|
NMR Spectra.mnova | 967KB | chemical/x-mnova | NMR Spectrum |
NMR Spectra.mnpub | 0 | chemical/x-mnpub | Mestrenova signature file for NMR Spectra.mnova |
IR Spectrum.pdf | 51KB | application/pdf | IR Spectrum |
Mass Spectrum.pdf | 83KB | application/pdf | Mass Spectrum |
HPLC (R)-Enantiomer.pdf | 58KB | application/pdf | HPLC (R)-Enantiomer |
HPLC (R)-Enantiomer Report.pdf | 11KB | application/pdf | HPLC (R)-Enantiomer Report |
HPLC Racemic.pdf | 59KB | application/pdf | HPLC Racemic |
HPLC Racemic Report.pdf | 12KB | application/pdf | HPLC Racemic Report |
Member of collection / collaboration
DOI | Description |
---|---|
10.14469/hpc/14345 | Fortuitous Enantiomeric Self-Rectification of an Unreported Partial Racemisation in the Synthesis of a Chiral Phosphoric Acid: A Warning to Practitioners |