(R)-(+)-3,3'-Di(phenanthren-9-yl)-[1,1'-binaphthalene]-2,2'-diol (5)
DOI: 10.14469/hpc/14351 Metadata
Created: 2024-06-18 13:49
Last modified: 2024-07-11 17:25
License: Creative Commons: Public Domain Dedication 1.0
Funding: (none given)
Description
NMR, IR, HRMS, and HPLC data for (R)-(+)-3,3'-di(phenanthren-9-yl)-[1,1'-binaphthalene]-2,2'-diol (5)
Files
| Filename | Size | Type | Description |
|---|---|---|---|
| NMR Spectra.mnova | 654KB | chemical/x-mnova | NMR Spectrum |
| NMR Spectra.mnpub | 0 | chemical/x-mnpub | Mestrenova signature file for NMR Spectra.mnova |
| IR Spectrum.pdf | 52KB | application/pdf | IR Spectrum |
| Mass Spectrum.pdf | 59KB | application/pdf | Mass Spectrum |
| HPLC (R)-Enantiomer (91-9 er).pdf | 106KB | application/pdf | HPLC (R)-Enantiomer (91:9 er) |
| HPLC (R)-Enantiomer.PDF | 74KB | application/octet-stream | HPLC (R)-Enantiomer (>99:1 er) (note, due to reconfiguration of the HPLC machine, a shift in retention times is observed) |
| HPLC Racemic.pdf | 108KB | application/pdf | HPLC Racemic |
Member of collection / collaboration
| DOI | Description |
|---|---|
| 10.14469/hpc/14345 | Fortuitous Enantiomeric Self-Rectification of an Unreported Partial Racemisation in the Synthesis of a Chiral Phosphoric Acid: A Warning to Practitioners |