2-formyl-6-methoxyphenyl oleate
DOI: 10.14469/hpc/10233 Metadata
Created: 2022-03-13 04:24
Last modified: 2022-03-13 12:14
License: Creative Commons: Public Domain Dedication 1.0
Funding: (none given)
Description
DMAP (0.06 g, 0.5 mmol) was mixed with EDC.HCl (1.25 g, 6.5 mmol) in acetonitrile (25 mL), added with ortho-vanillin and oleic acid. The mixture was heated under reflux for one hour and was monitored by TLC. It was extracted with haxane and ethyl acetate. The resulting product was then washed with 1 M aqueous HCl twice, aqueous NaHCO3 twice, water and NaCl twice. MgSO4 was added to dry it and and the solvent was removed with rotary evaporator. Finally 2-formyl-6-methoxyphenyl oleate was formed.
Files
| Filename | Size | Type | Description |
|---|---|---|---|
| 2-formyl-6-methoxyphenyl oleate.cdxml | 7KB | chemical/x-cdxml | chemdraw file |
| ss5121.mnova | 482KB | chemical/x-mnova | MestreNova data file |
| ss5121.mnpub | 0 | chemical/x-mnpub | Mestrenova signature file for ss5121.mnova |
| ss5121.jdx | 155KB | chemical/x-jcamp-dx | jdx data file |
| ss5121_PROTON.pdf | 383KB | application/pdf | pdf data file |
| ss5121_PROTON-1-1.jdf | 550KB | chemical/x-jeol-jdf | jdf data file |
| ss5121_PROTON-1-1.mnpub | 0 | chemical/x-mnpub | Mestrenova signature file for ss5121_PROTON-1-1.jdf |
Member of collection / collaboration
| DOI | Description |
|---|---|
| 10.14469/hpc/8679 | 1st Year undergraduate synthesis 1.2 laboratory (2021-2022) |
Subject Keywords
| Keyword | Value |
|---|---|
| inchi | InChI=1S/C26H40O4/c1-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-21-25(28)30-26-23(22-27)19-18-20-24(26)29-2/h10-11,18-20,22H,3-9,12-17,21H2,1-2H3/b11-10- |
| inchikey | UJCBTNJTWLPTOX-KHPPLWFESA-N |