Mestrelab Research S.L.v>%B$.AppleSystemUIFont@22{index}?$$.AppleSystemUIFont@22{name, 0}?nMestReNova14.0.0-23239UV/I˖nbZcZWZKd-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukCreate Item (Text)0|&%E8'<joshuadavies%s0^2 Text Item TypeTextr Type Report SpecialSubType Peaks,1HMetadatad-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukEdit text item0|&%E8'<joshuadavies%s0{  Peak Report

1H NMR (400 MHz, CDCl3) δ 7.36, 7.34, 7.32, 7.30, 7.29, 6.52, 5.47, 5.14, 5.11, 5.09, 5.07, 4.28, 4.26, 1.48, 1.47, 1.39, 1.37.

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 7.36, 7.34, 7.32, 7.30, 7.29, 6.52, 5.47, 5.14, 5.11, 5.09, 5.07, 4.28, 4.26, 1.48, 1.47, 1.39, 1.37.

d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukMove selection0|&%E8'<joshuadavies%s0~ Text Item TypeText @ x5860 @' y6439d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukEdit text item0|&%E8'<joshuadavies%s0)  Peak Report

1H NMR (400 MHz, CDCl3) δ 7.36, 7.34, 7.32, 7.30, 7.29, 6.52, 5.47, 5.14, 5.11, 5.09, 5.07, 4.28, 4.26, 1.48, 1.47, 1.39, 1.37.

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 7.36, 7.34, 7.32, 7.30, 7.29, 6.52, 5.47, 5.14, 5.11, 5.09, 5.07, 4.28, 4.26, 1.48, 1.47, 1.39, 1.37.

d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukEdit text item0|&%E8'<joshuadavies%s1J  Peak Report

1H NMR (400 MHz, CDCl3) δ 7.36 - 7.29 (m, 10H), 6.52 (br s, 1H), 5.47 (br s, 1H), 5.14, 5.11, 5.09, 5.07, 4.28, 4.26, 1.48, 1.47, 1.39, 1.37.

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 7.36 - 7.29 (m, 10H), 6.52 (br s, 1H), 5.47 (br s, 1H), 5.14, 5.11, 5.09, 5.07, 4.28, 4.26, 1.48, 1.47, 1.39, 1.37.

d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukEdit text item0|&%E8'<joshuadavies%s2YW  Peak Report

1H NMR (400 MHz, CDCl3) δ 7.36 - 7.29 (m, 10H), 6.52 (br s, 1H), 5.47 (br s, 1H), 5.09 (s, 3H), 4.28, 4.26, 1.48, 1.47, 1.39, 1.37.

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 7.36 - 7.29 (m, 10H), 6.52 (br s, 1H), 5.47 (br s, 1H), 5.09 (s, 3H), 4.28, 4.26, 1.48, 1.47, 1.39, 1.37.

d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukEdit text item0|&%E8'<joshuadavies%s3  Peak Report

1H NMR (400 MHz, CDCl3) δ 7.36 - 7.29 (m, 10H), 6.52 (br s, 1H), 5.47 (br s, 1H), 5.09 (s, 3H), 4.28 (br s, 1H), 4.26, 1.48, 1.47, 1.39, 1.37.

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 7.36 - 7.29 (m, 10H), 6.52 (br s, 1H), 5.47 (br s, 1H), 5.09 (s, 3H), 4.28 (br s, 1H), 4.26, 1.48, 1.47, 1.39, 1.37.

d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukEdit text item0|&%E8'<joshuadavies%s3  Peak Report

1H NMR (400 MHz, CDCl3) δ 7.36 - 7.29 (m, 10H), 6.52 (br s, 1H), 5.47 (br s, 1H), 5.09 (s, 3H), 4.28 (br s, 1H), 4.26, 1.48, 1.47, 1.39, 1.37.

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 7.36 - 7.29 (m, 10H), 6.52 (br s, 1H), 5.47 (br s, 1H), 5.09 (s, 3H), 4.28 (br s, 1H), 4.26, 1.48, 1.47, 1.39, 1.37.

d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukEdit text item0|&%E8'<joshuadavies%s4   Peak Report

1H NMR (400 MHz, CDCl3) δ 7.36 - 7.29 (m, 10H), 6.52 (br s, 1H), 5.47 (br s, 1H), 5.09 (s, 3H), 4.28 (br s, 1H), 1.48 - 1.47 (d, 3H, J = , 1.39, 1.37.

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 7.36 - 7.29 (m, 10H), 6.52 (br s, 1H), 5.47 (br s, 1H), 5.09 (s, 3H), 4.28 (br s, 1H), 1.48 - 1.47 (d, 3H, J = , 1.39, 1.37.

d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.uk#Edit text item0|&%E8'<joshuadavies%s4ž  Peak Report

1H NMR (400 MHz, CDCl3) δ 7.36 - 7.29 (m, 10H), 6.52 (br s, 1H), 5.47 (br s, 1H), 5.09 (s, 3H), 4.28 (br s, 1H), 1.48 - 1.47 (d, 3H, J = 6.89 Hz), 1.39 - 1.37 (d, 3H, J = 6.89 Hz).

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 7.36 - 7.29 (m, 10H), 6.52 (br s, 1H), 5.47 (br s, 1H), 5.09 (s, 3H), 4.28 (br s, 1H), 1.48 - 1.47 (d, 3H, J = 6.89 Hz), 1.39 - 1.37 (d, 3H, J = 6.89 Hz).

e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localDelete Item (Text)0|&%E8'<joshuadavies%o Text Item TypeTextd-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukCreate Item (Text)wʅkGOu joshuadavies%s6 Text Item TypeTextt Type Report SpecialSubType Peaks,13CMetadatad-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukEdit text itemwʅkGOu joshuadavies%s6  Peak Report

13C NMR (101 MHz, CDCl3) δ 171.26, 156.04, 142.93, 136.17, 128.71, 128.59, 128.27, 128.06, 127.40, 126.04, 67.04, 50.57, 48.85, 21.83, 18.62.

Text Peak Report

13C NMR (101 MHz, CDCl3) δ 171.26, 156.04, 142.93, 136.17, 128.71, 128.59, 128.27, 128.06, 127.40, 126.04, 67.04, 50.57, 48.85, 21.83, 18.62.

d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukMove selectionwʅkGOu joshuadavies%s6C Text Item TypeText @ x5321 @} y6269d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukEdit text itemwʅkGOu joshuadavies%s6  Peak Report

13C NMR (101 MHz, CDCl3) δ 171.26, 156.04, 142.93, 136.17, 128.71, 128.59, 128.27, 128.06, 127.40, 126.04, 67.04, 50.57, 48.85, 21.83, 18.62.

Text Peak Report

13C NMR (101 MHz, CDCl3) δ 171.26, 156.04, 142.93, 136.17, 128.71, 128.59, 128.27, 128.06, 127.40, 126.04, 67.04, 50.57, 48.85, 21.83, 18.62.

e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localDelete Item (Text)wʅkGOu joshuadavies%p  Text Item TypeTextG: (#GG=% p(66@'>|@r66 (#pFObΡ#d-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukx Create Pagea@CMjoshuadavies%n1t/  At11d-  MestReNovaZ macOS 10.16dyn3158-14.wlan.ic.ac.ukv Paste Pagea@CMjoshuadavies%U2  At2(66@'>|@r66 (#a@CMҗҏ҇m[ (@o0JKyyyyyyyyyLd-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukDImport Item (NMR Spectrum)jpO|OR>z. joshuadavies%n1t$ NMR Spectrum Item Type NMR Spectrum Filename T/Volumes/Av400A/brad/nmr/Oct14-2021/10/fidMetadatad-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukr ProcessingjpO|OR>z. joshuadavies%n1uL PCf1zero@V앿 first@2(j+ Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321?ᙙ Parametersd-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukDecrease IntensityjpO|OR>z. joshuadavies%n1+ [-1635.59, 18017.1] Scale[-1635.59, 18017.1]d-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukManual IntegrationjpO|OR>z. joshuadavies%n1 ppmUnitsppmR 1To@O 7Fromz Integralsd-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukZoomjpO|OR>z. joshuadavies%n1. [-0.00521958, 8.71601]( Horizontal[-0.00521958, 8.71601]+ [-1635.59, 18017.1]#Vertical[-1635.59, 18017.1]d-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukIncrease IntensityjpO|OR>z. joshuadavies%n1+ [-1478.84, 16290.3] Scale[-1478.84, 16290.3]d-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukManual Peak PickingjpO|OR>z. joshuadavies%n1VD To?#FpߚFrom@M[rRegion @aL# Threshold2177.5026990796086 "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method StandardParamsd-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukManual Peak PickingjpO|OR>z. joshuadavies%n1D To@ ,ě>From@ R]bRegion @k,v# Threshold217.39264196057593 "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method StandardParamsd-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukManual Peak PickingjpO|OR>z. joshuadavies%n1D To@äFrom@ -*Region @XNt# Threshold99.786038533433384 "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method StandardParamsd-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukManual IntegrationjpO|OR>z. joshuadavies%n1 ppmUnitsppmR 1To?Z?JtFrom?wU Integralsd-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukManual IntegrationjpO|OR>z. joshuadavies%n2 ppmUnitsppmR 1To@~ɼFrom@=K Integralsd-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukManual IntegrationjpO|OR>z. joshuadavies%n2 I ppmUnitsppmR 1To@4From@ ,O\ Integralsd-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukManual IntegrationjpO|OR>z. joshuadavies%n2 ppmUnitsppmR 1To@6MnFrom@[mt Integralsd-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukEdit IntegralsjpO|OR>z. joshuadavies%nv`0Norm ValueA!Norm Value@ Integralsd-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.uktDelete IntegralsjpO|OR>z. joshuadavies%ne 1UUID &{9bad6928-23eb-44e2-8aef-d9b114c0d695}Regions1To?wUFrom?Z?JvMode ManualMaximumA!AreaA! Integralsd-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukZoomjpO|OR>z. joshuadavies%nz) [0.476824, 1.752]# Horizontal[0.476824, 1.752]+ [-1478.84, 16290.3]#Vertical[-1478.84, 16290.3]d-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukManual IntegrationjpO|OR>z. joshuadavies%n/ ppmUnitsppmR 1To?rUjFrom?w Integralsd-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukManual IntegrationjpO|OR>z. joshuadavies%n ppmUnitsppmR 1To?T']eBFrom? Integralsd-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.uk Full Zoom OutjpO|OR>z. joshuadavies%nV+ [-4.00577, 16.0058]% Horizontal[-4.00577, 16.0058]+ [-1478.84, 16290.3]#Vertical[-1478.84, 16290.3]d-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukZoomjpO|OR>z. joshuadavies%n%* [3.80362, 8.08541]$ Horizontal[3.80362, 8.08541]+ [-1478.84, 16290.3]#Vertical[-1478.84, 16290.3]d-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukManual IntegrationjpO|OR>z. joshuadavies%n>w ppmUnitsppmR 1To@Q|From@ Integralsd-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukManual IntegrationjpO|OR>z. joshuadavies%nF ppmUnitsppmR 1To@`xFrom@aÑ Integralsd-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.uk Full Zoom OutjpO|OR>z. joshuadavies%nK+ [-4.00577, 16.0058]% Horizontal[-4.00577, 16.0058]+ [-1478.84, 16290.3]#Vertical[-1478.84, 16290.3]d-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukZoomjpO|OR>z. joshuadavies%nUs+ [0.183961, 8.36918]% Horizontal[0.183961, 8.36918]+ [-1478.84, 16290.3]#Vertical[-1478.84, 16290.3]d-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukIncrease IntensityjpO|OR>z. joshuadavies%nXw+ [-1403.96, 15465.5] Scale[-1403.96, 15465.5]d-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukIncrease IntensityjpO|OR>z. joshuadavies%nY( [-1337.1, 14729]Scale[-1337.1, 14729]d-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukIncrease IntensityjpO|OR>z. joshuadavies%nYw+ [-1273.43, 14027.6] Scale[-1273.43, 14027.6]d-  MestReNovaZ macOS 10.16dyn3150-40.wlan.ic.ac.ukIncrease IntensityjpO|OR>z. joshuadavies%nY+ [-1212.79, 13359.7] Scale[-1212.79, 13359.7]e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukDecrease IntensityjpO|OR>z. joshuadavies%o5n+ [-1517.99, 16721.6] Scale[-1517.99, 16721.6]e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukIncrease IntensityjpO|OR>z. joshuadavies%o6* [-81.1049, 893.42]Scale[-81.1049, 893.42]e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukDecrease IntensityjpO|OR>z. joshuadavies%o6 F+ [-861.154, 9486.14] Scale[-861.154, 9486.14]e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.uk Full Zoom OutjpO|OR>z. joshuadavies%o6 + [-4.00577, 16.0058]% Horizontal[-4.00577, 16.0058]+ [-861.154, 9486.14]#Vertical[-861.154, 9486.14]e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukDecrease IntensityjpO|OR>z. joshuadavies%o6I+ [-1734.66, 19108.3] Scale[-1734.66, 19108.3]e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukZoomjpO|OR>z. joshuadavies%o6+ [0.467732, 8.24306]% Horizontal[0.467732, 8.24306]+ [-1734.66, 19108.3]#Vertical[-1734.66, 19108.3]e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukZoomjpO|OR>z. joshuadavies%o6* [0.84849, 8.04214]$ Horizontal[0.84849, 8.04214]+ [-1734.66, 19108.3]#Vertical[-1734.66, 19108.3]e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukIncrease IntensityjpO|OR>z. joshuadavies%o6+ [-1173.56, 12927.4] Scale[-1173.56, 12927.4]e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukDecrease IntensityjpO|OR>z. joshuadavies%o6O* [-1418.7, 15627.8]Scale[-1418.7, 15627.8]e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukIncrease IntensityjpO|OR>z. joshuadavies%o9+ [-1210.16, 13330.6] Scale[-1210.16, 13330.6]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.uk Edit IntegraljpO|OR>z. joshuadavies%s.L{2298b426-d316-41c0-9a16-579751ec1f4d}Regions1To@Maximum@Area@L{2298b426-d316-41c0-9a16-579751ec1f4d}Regions1To@cMaximum@i6Area@i6 Integralsd-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.uk Edit IntegraljpO|OR>z. joshuadavies%s..L{2298b426-d316-41c0-9a16-579751ec1f4d}Regions1From@Q|Maximum@i6Area@i6L{2298b426-d316-41c0-9a16-579751ec1f4d}Regions1From@~ j|tMaximum@kw"Area@kw" Integralsd-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.uk Full Zoom OutjpO|OR>z. joshuadavies%s.8+ [-4.00577, 16.0058]% Horizontal[-4.00577, 16.0058]+ [-1210.16, 13330.6]#Vertical[-1210.16, 13330.6]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukZoomjpO|OR>z. joshuadavies%s.- [-0.0367497, 8.77907]' Horizontal[-0.0367497, 8.77907]+ [-1210.16, 13330.6]#Vertical[-1210.16, 13330.6]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukIncrease IntensityjpO|OR>z. joshuadavies%s/+ [-959.163, 10565.8] Scale[-959.163, 10565.8]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukDecrease IntensityjpO|OR>z. joshuadavies%s/ + [-1169.57, 12883.5] Scale[-1169.57, 12883.5]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.uk nDelete All PeaksjpO|OR>z. joshuadavies%s/  18w1? t _ f1?hUUID`5JVIb 8LType CompoundMode ManualIntensity@ f17w1?~̭.f1?BMxUUIDېIT$l^Type CompoundMode ManualIntensity@ "c 16w1?L%ef1?z;\UUID`\M7GPsIZType CompoundMode ManualIntensity@*15w1?)췶f1?A0UUID Ba>Type CompoundMode ManualIntensity@&,~14w1?|]J4af1@F DUUIDV"8D *a:Type CompoundMode ManualIntensity@tM 13w1?ӄ2Jf1@ "-IUUIDxygG}Type CompoundMode ManualIntensity@vvA12w1?sv:=f1@]LMUUIDj'L.Y# Type CompoundMode ManualIntensity@}:J2311w1?LTf1@F Fy-UUID56H?9"WʴType CompoundMode ManualIntensity@n: z10w1?W,f1@WΣN}UUID"U B/HType CompoundMode ManualIntensity@:r09w1?nDf1@o7UUID<_KnFH"ΔType CompoundMode ManualIntensity@5ވ08w1?2 Yf1@JUUID_9JJ5Type CompoundMode ManualIntensity@uBr207w1?.f1@޼UUIDY9E9F ЪVType CompoundMode ManualIntensity@{06w1? Kdf1@}%UUID^"O@HVType CompoundMode ManualIntensity@xkM05w1?WZvf1@'}UUID_S B'L GType CompoundMode ManualIntensity@φ]104w1??g8f1@2FUUIDn_FLerE Type CompoundMode ManualIntensity@mr03w1?;%~f1@Cr4{UUID8SNz$"^4Type CompoundMode ManualIntensity@G 02w1?2Qf1@\6=UUID L]J+ֵType CompoundMode ManualIntensity@ B801w1?jcf1@uCUUIDŜ`IQAfType CompoundMode ManualIntensity@XEb Peaksd-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.uk0 Delete PeaksjpO|OR>z. joshuadavies%s/( 1w1?|]J4af1@F DUUIDV"8D *a:Type CompoundMode ManualIntensity@tM Peaksd-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukZoomjpO|OR>z. joshuadavies%s1Q`* [5.00094, 5.31764]$ Horizontal[5.00094, 5.31764]+ [-1169.57, 12883.5]#Vertical[-1169.57, 12883.5]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.uk0 Delete PeaksjpO|OR>z. joshuadavies%s1wH 1w1?2 Yf1@JUUID_9JJ5Type CompoundMode ManualIntensity@uBr2 Peaksd-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.uk Delete PeaksjpO|OR>z. joshuadavies%s1| 2w1?LTf1@F Fy-UUID56H?9"WʴType CompoundMode ManualIntensity@n: z1w1?W,f1@WΣN}UUID"U B/HType CompoundMode ManualIntensity@:r Peaksd-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.uk Full Zoom OutjpO|OR>z. joshuadavies%s1+ [-4.00577, 16.0058]% Horizontal[-4.00577, 16.0058]+ [-1169.57, 12883.5]#Vertical[-1169.57, 12883.5]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukZoomjpO|OR>z. joshuadavies%s1, [-0.383581, 7.80794]& Horizontal[-0.383581, 7.80794]+ [-1169.57, 12883.5]#Vertical[-1169.57, 12883.5]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukDecrease IntensityjpO|OR>z. joshuadavies%s1m+ [-1509.28, 16625.7] Scale[-1509.28, 16625.7]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.uk Peak PickingjpO|OR>z. joshuadavies%s1 "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard Parametersd-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukZoomjpO|OR>z. joshuadavies%s2`q* [4.10377, 4.43934]$ Horizontal[4.10377, 4.43934]+ [-1509.28, 16625.7]#Vertical[-1509.28, 16625.7]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukIncrease IntensityjpO|OR>z. joshuadavies%s2+ [-206.018, 2269.42] Scale[-206.018, 2269.42]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.uk0 Delete PeaksjpO|OR>z. joshuadavies%s2՜ 1w1?ӄ2Jf1@ "-IUUIDxygG}Type CompoundMode ManualIntensity@vvA Peaksd-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukDecrease IntensityjpO|OR>z. joshuadavies%s22+ [-254.406, 2802.44] Scale[-254.406, 2802.44]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.uk Full Zoom OutjpO|OR>z. joshuadavies%s3+ [-4.00577, 16.0058]% Horizontal[-4.00577, 16.0058]+ [-254.406, 2802.44]#Vertical[-254.406, 2802.44]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukZoomjpO|OR>z. joshuadavies%s33* [2.17036, 6.23144]$ Horizontal[2.17036, 6.23144]+ [-254.406, 2802.44]#Vertical[-254.406, 2802.44]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukDecrease IntensityjpO|OR>z. joshuadavies%s3#+ [-711.539, 7838.04] Scale[-711.539, 7838.04]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukZoomjpO|OR>z. joshuadavies%s3** [4.05591, 4.49741]$ Horizontal[4.05591, 4.49741]+ [-711.539, 7838.04]#Vertical[-711.539, 7838.04]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukIncrease IntensityjpO|OR>z. joshuadavies%s3.L+ [-260.218, 2866.46] Scale[-260.218, 2866.46]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.uk Full Zoom OutjpO|OR>z. joshuadavies%s3o+ [-4.00577, 16.0058]% Horizontal[-4.00577, 16.0058]+ [-260.218, 2866.46]#Vertical[-260.218, 2866.46]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukDecrease IntensityjpO|OR>z. joshuadavies%s3* [-693.335, 7637.5]Scale[-693.335, 7637.5]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukZoomjpO|OR>z. joshuadavies%s3, [-0.572762, 2.01271]& Horizontal[-0.572762, 2.01271]* [-693.335, 7637.5]"Vertical[-693.335, 7637.5]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.uk Full Zoom OutjpO|OR>z. joshuadavies%s3+ [-4.00577, 16.0058]% Horizontal[-4.00577, 16.0058]* [-693.335, 7637.5]"Vertical[-693.335, 7637.5]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukZoomjpO|OR>z. joshuadavies%s4+ [-0.16287, 2.01271]% Horizontal[-0.16287, 2.01271]* [-693.335, 7637.5]"Vertical[-693.335, 7637.5]d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukZoomjpO|OR>z. joshuadavies%s4) [1.07691, 1.6521]# Horizontal[1.07691, 1.6521]* [-693.335, 7637.5]"Vertical[-693.335, 7637.5]d-  MestReNovaZ macOS 10.16dyn3154-95.wlan.ic.ac.uk Full Zoom OutjpO|OR>z. joshuadavies%Cws+ [-4.00577, 16.0058]% Horizontal[-4.00577, 16.0058]* [-693.335, 7637.5]"Vertical[-693.335, 7637.5]d-  MestReNovaZ macOS 10.16dyn3154-95.wlan.ic.ac.ukDecrease IntensityjpO|OR>z. joshuadavies%C}y+ [-1066.19, 11744.7] Scale[-1066.19, 11744.7]d-  MestReNovaZ macOS 10.16dyn3154-95.wlan.ic.ac.ukZoomjpO|OR>z. joshuadavies%C , [0.0767587, 8.48269]& Horizontal[0.0767587, 8.48269]+ [-1066.19, 11744.7]#Vertical[-1066.19, 11744.7]d-  MestReNovaZ macOS 10.16dyn3154-95.wlan.ic.ac.ukDecrease IntensityjpO|OR>z. joshuadavies%CM) [-1288.08, 14189]Scale[-1288.08, 14189]d-  MestReNovaZ macOS 10.16dyn3154-95.wlan.ic.ac.ukIncrease IntensityjpO|OR>z. joshuadavies%Ce+ [-1045.18, 11513.3] Scale[-1045.18, 11513.3]e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.local Full Zoom OutjpO|OR>z. joshuadavies%o}+ [-4.00577, 16.0058]% Horizontal[-4.00577, 16.0058]+ [-1045.18, 11513.3]#Vertical[-1045.18, 11513.3]e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localZoomjpO|OR>z. joshuadavies%o, [-0.976347, 8.99347]& Horizontal[-0.976347, 8.99347]+ [-1045.18, 11513.3]#Vertical[-1045.18, 11513.3]e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localIncrease IntensityjpO|OR>z. joshuadavies%ow) [-942.031, 10377]Scale[-942.031, 10377]1D1HjpO|OR>z. `*qHh@@Q?@ NMR SpectrumNMR@@@@W@0 u]XP, vD}@j&L2e.SF NS Text@>2MNova Default4,Orange-Cyan (Gradient) UBϐ}CrYM78"|mUUnqǹ*@:8U~NXnJwF^=:?^=1?nJwF?~NTz?@:Q?f(?"|m?YM/?ϐ}C@? 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T/Volumes/Av400A/brad/nmr/Oct14-2021/10/fidData File Name =brukerExpName(datafile(_FILEPATH_), parm.txt(NAME), parm.txt(EXPNO), parm.txt(PROCNO))"Oct14-2021.10.fid Title *=Str.trimStr(title())jd-317 hComment  acqus ORIGIN&Bruker BioSpin GmbH Origin  acqus OWNERnmr Owner Site  acqus$INSTRUM spectInstrument  Author  acqus$SOLVENT CDCl3Solvent  acqus$TE293.516Temperature  acqus$PULPROGzg30Pulse Sequence L=brukerExperimentType(acqus($PULPROG))1DExperiment  acqus$PROBHDT5 mm PABBO BB/19F-1H/D Z-GRD Z108618/0624 Probe  acqus$NS16Number of Scans  acqus$RG 142.31Receiver Gain  acqus $D[1]1 Relaxation Delay  acqus $P[1] 11.25Pulse Width  =brukerPresatFreq(acqus($PULPROG), acqus($SPOFFS[6]), acqus($SFO1), acqus($O1), acqus($SW), procs($OFFSET), fq0list()) .Presaturation Frequency j=brukerAQ(parm.txt(AQ;;;1), acqus($SW_h), acqus($TD))2.0447233 Acquisition Time v=brukerDate2(acqus($DATE), parm.txt(Date_), parm.txt(Time))&2021-10-14T14:43:00 Acquisition Date  acqus_LASTMODIFIED_&2021-10-14T14:43:10"Modification Date  Class   %100 Purity  0 Spectrum Quality 400.41240246,Spectrometer Frequency  8012.82051282051Spectral Width "-1603.95025642547 Lowest Frequency 1HNucleus .=Utl.div(acqus($TD), 2) 16384Acquired Size  65536Spectral Size  "0.122265938000801 $Digital Resolution $Absolute Reference/ uxnmr.par%n(%n'%n. 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T/Volumes/Av400A/brad/nmr/Oct14-2021/11/fidData File Name =brukerExpName(datafile(_FILEPATH_), parm.txt(NAME), parm.txt(EXPNO), parm.txt(PROCNO))"Oct14-2021.11.fid Title *=Str.trimStr(title())jd-317 cComment  acqus ORIGIN&Bruker BioSpin GmbH Origin  acqus OWNERnmr Owner Site  acqus$INSTRUM spectInstrument  Author  acqus$SOLVENT CDCl3Solvent  acqus$TE294.6259Temperature  acqus$PULPROG zgpg30Pulse Sequence L=brukerExperimentType(acqus($PULPROG))1DExperiment  acqus$PROBHDT5 mm PABBO BB/19F-1H/D Z-GRD Z108618/0624 Probe  acqus$NS480Number of Scans  acqus$RG 207.33Receiver Gain  acqus $D[1]1 Relaxation Delay  acqus $P[1]9.6Pulse Width  =brukerPresatFreq(acqus($PULPROG), acqus($SPOFFS[6]), acqus($SFO1), acqus($O1), acqus($SW), procs($OFFSET), fq0list()) .Presaturation Frequency j=brukerAQ(parm.txt(AQ;;;1), acqus($SW_h), acqus($TD))0.6225920 Acquisition Time v=brukerDate2(acqus($DATE), parm.txt(Date_), parm.txt(Time))&2021-10-14T15:29:00 Acquisition Date  acqus_LASTMODIFIED_&2021-10-14T15:29:41"Modification Date  Class   %100 Purity  0 Spectrum Quality  100.694248477066,Spectrometer Frequency  26315.7894736842Spectral Width "-2084.41767085039 Lowest Frequency 13CNucleus .=Utl.div(acqus($TD), 2) 16384Acquired Size  65536Spectral Size  "0.401547080592105 $Digital Resolution $Absolute Reference3 uxnmr.par%nS*p%nFh%s3 X`x\Ys6~&ڵRR(q#J IٞyIic O[!ՙz#_¡mM+OU^;L̍-i5K Ӂeږm[-ocd}W nyfX"x݊\.+ZQzs!DFLy~e¤uq}w d8` c"cpQ-Q8UDԇrl)hafº(M&Zẅ́7Qmϟ_YMJ~N2aJK%J<:O rt@X;Di퐣cCvHRCյJ4u{lh{lzDi(a2>ʵ:0}}=2iK{XڣȮ'B"I Ud"YzE6*rjPJ˘ #iyQH48H&>ZQQ#*r1dQ-ãxǻL֏?UaJTXwWO޾T= YH9/a\.X'Ԡz2(,zĊ>ir+jZnVRJ%eؠTjRkBjMH 7!&ф7! 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? ? ? ? ? ? ?r b?:2ޗB,:?(:>. &֕?6C-@I???@& ?6C-?@$@$?@.@.@$ *@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{* r SJB";@ h: !  !  @4@( =# <?ٙ-? ?@?@?d??zG{6,vq[VJ @r@@UnknownCDzd@ (\)@ =p @M@N?tzG{(@YAׄ@9%u*DSS methyl signal D2O@Y@Y@Y@Y@Yr b?:2,:?(:>. &֕?6C-@I???@& ?6C-?@@$?@.@.@$ & ?6C-??@Y?d 2D$????zG{8# # # # # # #               h: ! ) ! ) @4@(=# <????zG{??????????bD0$?@Y?zG{h: !  !  @4@( =# <?ٙC@@U???????h: ! ) ! ) @4@( =# =L_!@???ffffff?@V??ffffff?????????333333_!@???ffffff@@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333       l_Z% a\^m?}% ^m?}^m?}@SC5I5a\% _Z% _Z% _Z% _Z%   ?Ee0  !de0 4P@nlC !de0  !de0  !de0  !de0  !de0  !d? ? ? ? ? ? ? ?r b?:2ޗB,:?(:>. &֕?6C-@I???@& ?6C-?@$@$?@.@.@$ *@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{&7(1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard yK`NryL@nlu4т@ehs5J@U¾˜?B0Dža?B0Dža1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardyOCw]j@nlu4т@c;4wS@;}be?qάY?qάY1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard:z@{Fޔ4θ@nlu4т@aDFW@Jp'?9?91,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard7 ABDž@nlu4т@ap[@>|-/>?f!D?f!D1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standardd+Fa@ @nlu4т@`9@tX/S?z8`Y?z8`Y1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard֯@nlu4т@`<@rhbg?޲3O?޲3O1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardgWI۽vJM4@nlu4т@`{I+z@g%UX#?%q ?%q 1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard뱱C,D ^@nlu4т@`}@rQʨX?YemZ?YemZ1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standardl0# E€6@@nlu4т@_ٝ1@fdV?ƭ [?ƭ [1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardڭDɿ|t[ s@nlu4т@_GWL;@s>1)?m/$?m/$1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard 5pKɟ@*@nlu4т@Pb@T6?T 0k0?T 0k01,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard_MJҠ \V>@nlu4т@IH`fF<@OC <?N?N1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardFFNkya|@nlu4т@Hl]T@^=E?һ?һ1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standarde[xMyE@nlu4т@56<=@Y?q}2?q}21,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standardc߉CGϏZt@nlu4т@2֛He@R(h?_h?_h T/Volumes/Av400A/brad/nmr/Oct14-2021/11/fid