Mestrelab Research S.L.=B$.AppleSystemUIFont@22{index}?$$.AppleSystemUIFont@22{name, 0}?e-  MestReNovaZ macOS 10.16dyn3146-243.wlan.ic.ac.ukZDocument Items ParentshipHVE)cF]joshuadavies%0onMestReNova14.0.0-23239HVE)cF] e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukCreate Item (Text)_w9G\uPjoshuadavies%ot Text Item TypeTextt Type Report SpecialSubType Peaks,13CMetadatae-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukMove selection_w9G\uPjoshuadavies%o|S Text Item TypeText @ x5326 @ y6099e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukEdit text item_w9G\uPjoshuadavies%o3  Peak Report

13C NMR (101 MHz, CDCl3) δ 170.04, 139.12, 137.62, 132.14, 129.80, 129.04, 128.72, 124.47, 119.97, 39.21, 30.79.

Text Peak Report

13C NMR (101 MHz, CDCl3) δ 170.04, 139.12, 137.62, 132.14, 129.80, 129.04, 128.72, 124.47, 119.97, 39.21, 30.79.

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Һ)?N!@#ua\% _Z% _Z% _Z% _Z%   ?Ee0  !de0  H@04 !de0  !de0  !de0  !de0  !de0  !d? ? ? ? ? ? ? ?r b?:2ޗB,:?(:>. &֕?6C-@I???@& ?6C-?@$@$?@.@.@$ *@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{* n OF>;@ h: !  !  @4@( =# <?ٙ-? ?@?@?d??zG{6,vq[VJ @r@@UnknownCDzd@ (\)@ =p @M@N?tzG{(@YAׄ@Y&Me4Si CDCl3,  = 1%@Y@Y@Y@Y@Yr b?:2R,:?(:>. &֕?6C-@I???@& ?6C-?@@$?@.@.@$ & ?6C-??@Y?d 2D$????zG{8# # # # # # #               h: ! ) ! ) @4@(=# <????zG{??????????bD0$?@Y?zG{h: !  !  @4@( =# <?ٙC@@U???????h: ! ) ! ) @4@( =# =L_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?333333@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333       l_Z% a\ Һ)?N!%  Һ)?N! Һ)?N!@#ua\% _Z% _Z% _Z% _Z%   ?Ee0  !de0  H@04 !de0  !de0  !de0  !de0  !de0  !d? ? ? ? ? ? ? ?r b?:2ޗB,:?(:>. &֕?6C-@I???@& ?6C-?@$@$?@.@.@$ *@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{0[(1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardHc@ Ll<~=@07)u Hw@'Y_}@嵴u?t"D6y?t"D6y1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard |MK}U@07)u Hw@Ux@_j?sO W?sO W1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardXAҘzM s@07)u Hw@aGJO@VL?ge?ge1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standardv(ʑ@M{ev@07)u Hw@M䥮@e ?p2|F?p2|F1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard z.Ce#07@07)u Hw@8t872@(?mB?mB1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard T@RFq@07)u Hw@#^N@9vr?Y yU?Y yU1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard?3êRFǐ\na@07)u Hw@C)@+BcY?gݨ:f?gݨ:f1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard(/S4\K~P@07)u Hw@q@ЪK?at'1!?at'1!1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard2D_@07)u Hw@q@[nV@]T?kx+Ń8?kx+Ń81,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardQE^C䣞@07)u Hw@JPRL@G6G.G e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukCreate Item (Text)!+pM=0)Yrjoshuadavies%o& Text Item TypeTextr Type Report SpecialSubType Peaks,1HMetadatae-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukMove selection!+pM=0)Yrjoshuadavies%oE% Text Item TypeText @ x6050 @ y6379e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukEdit text item!+pM=0)Yrjoshuadavies%o!  Peak Report

1H NMR (400 MHz, CDCl3) δ 7.48 - 7.46 (d, 2H, , 7.34, 7.33, 7.31, 7.29, 7.27, 7.26, 7.22, 7.19, 7.17, 7.15, 7.13, 3.06, 3.04, 3.02, 2.66, 2.65, 2.63.

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 7.48 - 7.46 (d, 2H, , 7.34, 7.33, 7.31, 7.29, 7.27, 7.26, 7.22, 7.19, 7.17, 7.15, 7.13, 3.06, 3.04, 3.02, 2.66, 2.65, 2.63.

e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukEdit text item!+pM=0)Yrjoshuadavies%o  Peak Report

1H NMR (400 MHz, CDCl3) δ 7.48 - 7.46 (d, 2H, J = 7.79 Hz), 7.34, 7.33, 7.31, 7.29, 7.27, 7.26, 7.22, 7.19, 7.17, 7.15, 7.13, 3.06, 3.04, 3.02, 2.66, 2.65, 2.63.

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 7.48 - 7.46 (d, 2H, J = 7.79 Hz), 7.34, 7.33, 7.31, 7.29, 7.27, 7.26, 7.22, 7.19, 7.17, 7.15, 7.13, 3.06, 3.04, 3.02, 2.66, 2.65, 2.63.

e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukEdit text item!+pM=0)Yrjoshuadavies%oX.  Peak Report

1H NMR (400 MHz, CDCl3) δ 7.48 - 7.46 (d, 2H, J = 7.79 Hz), 7.35 - 7.26 (m, 4H), 7.22 - 7.13 (m, 4H), 3.06, 3.04, 3.02, 2.66, 2.65, 2.63.

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 7.48 - 7.46 (d, 2H, J = 7.79 Hz), 7.35 - 7.26 (m, 4H), 7.22 - 7.13 (m, 4H), 3.06, 3.04, 3.02, 2.66, 2.65, 2.63.

e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukEdit text item!+pM=0)Yrjoshuadavies%oF  Peak Report

1H NMR (400 MHz, CDCl3) δ 7.48 - 7.46 (d, 2H, J = 7.79 Hz), 7.35 - 7.26 (m, 4H), 7.22 - 7.13 (m, 4H), 3.06 - 3.02 (t, 2H, , 2.66, 2.65, 2.63.

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 7.48 - 7.46 (d, 2H, J = 7.79 Hz), 7.35 - 7.26 (m, 4H), 7.22 - 7.13 (m, 4H), 3.06 - 3.02 (t, 2H, , 2.66, 2.65, 2.63.

e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukEdit text item!+pM=0)Yrjoshuadavies%o)   Peak Report

1H NMR (400 MHz, CDCl3) δ 7.48 - 7.46 (d, 2H, J = 7.79 Hz), 7.35 - 7.26 (m, 4H), 7.22 - 7.13 (m, 4H), 3.06 - 3.02 (t, 2H, J = 7.7 Hz) , 2.66, 2.65, 2.63.

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 7.48 - 7.46 (d, 2H, J = 7.79 Hz), 7.35 - 7.26 (m, 4H), 7.22 - 7.13 (m, 4H), 3.06 - 3.02 (t, 2H, J = 7.7 Hz) , 2.66, 2.65, 2.63.

e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukEdit text item!+pM=0)Yrjoshuadavies%oW8  Peak Report

1H NMR (400 MHz, CDCl3) δ 7.48 - 7.46 (d, 2H, J = 7.79 Hz), 7.35 - 7.26 (m, 4H), 7.22 - 7.13 (m, 4H), 3.06 - 3.02 (t, 2H, J = 7.70 Hz) , 2.66, 2.65, 2.63.

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 7.48 - 7.46 (d, 2H, J = 7.79 Hz), 7.35 - 7.26 (m, 4H), 7.22 - 7.13 (m, 4H), 3.06 - 3.02 (t, 2H, J = 7.70 Hz) , 2.66, 2.65, 2.63.

e-  MestReNovaZ macOS 10.16dyn3158-227.wlan.ic.ac.ukEdit text item!+pM=0)Yrjoshuadavies%o  Peak Report

1H NMR (400 MHz, CDCl3) δ 7.48 - 7.46 (d, 2H, J = 7.79 Hz), 7.35 - 7.26 (m, 4H), 7.22 - 7.13 (m, 4H), 3.06 - 3.02 (t, 2H, J = 7.70 Hz) , 2.66 - 2.63 (t, 2H, J = 7.70 Hz).

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 7.48 - 7.46 (d, 2H, J = 7.79 Hz), 7.35 - 7.26 (m, 4H), 7.22 - 7.13 (m, 4H), 3.06 - 3.02 (t, 2H, J = 7.70 Hz) , 2.66 - 2.63 (t, 2H, J = 7.70 Hz).

d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukMove selection!+pM=0)Yrjoshuadavies%s  Text Item TypeText @ x5296 @s y6259d-  MestReNovaZ macOS 10.16dyn3151-79.wlan.ic.ac.ukEdit text item!+pM=0)Yrjoshuadavies%s  Peak Report

1H NMR (400 MHz, CDCl3) δ 7.48 - 7.46 (d, 2H, J = 7.79 Hz), 7.35 - 7.26 (m, 4H), 7.22 - 7.13 (m, 4H), 3.06 - 3.02 (t, 2H, J = 7.70 Hz) , 2.66 - 2.63 (t, 2H, J = 7.70 Hz).

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 7.48 - 7.46 (d, 2H, J = 7.79 Hz), 7.35 - 7.26 (m, 4H), 7.22 - 7.13 (m, 4H), 3.06 - 3.02 (t, 2H, J = 7.70 Hz) , 2.66 - 2.63 (t, 2H, J = 7.70 Hz).

Report SpecialPeaks,1H!+pM=0)Yr!+pM=0)Yr@@s?P?@Text@@s@@MA<!DOCTYPE HTML PUBLIC "-//W3C//DTD HTML 4.0//EN" "http://www.w3.org/TR/REC-html40/strict.dtd"> <html><head><meta name="qrichtext" content="1" /><meta http-equiv="Content-Type" content="text/html; charset=utf-8" /><title>Peak Report</title><style type="text/css"> p, li { white-space: pre-wrap; } </style></head><body style=" font-family:'.AppleSystemUIFont'; font-size:12pt; font-weight:400; font-style:normal;"> <p style=" margin-top:0px; margin-bottom:0px; margin-left:0px; margin-right:0px; -qt-block-indent:0; text-indent:0px;"><span style=" font-family:'Times New Roman'; font-size:10pt; vertical-align:super;">1</span><span style=" font-family:'Times New Roman'; font-size:10pt;">H NMR (400 MHz, CDCl</span><span style=" font-family:'Times New Roman'; font-size:10pt; vertical-align:sub;">3</span><span style=" font-family:'Times New Roman'; font-size:10pt;">)  7.48 - 7.46 (d, 2H, J = 7.79 Hz), 7.35 - 7.26 (m, 4H), 7.22 - 7.13 (m, 4H), 3.06 - 3.02 (t, 2H, J = 7.70 Hz) , 2.66 - 2.63 (t, 2H, J = 7.70 Hz).</span></p></body></html>@@@@! e-  MestReNovaZ macOS 10.16dyn3146-243.wlan.ic.ac.ukw Create Page\_OڐxC>joshuadavies%0/  At3l(66@'>|@r66 (#̒\_OڐxC>lllm[ (@o0JKume]UA e-  MestReNovaZ macOS 10.16dyn3146-243.wlan.ic.ac.ukDImport Item (NMR Spectrum)9K O<wjoshuadavies%0$ NMR Spectrum Item Type NMR Spectrum Filename T/Volumes/Av400C/brad/nmr/Jul13-2021/31/fidMetadatae-  MestReNovaZ macOS 10.16dyn3146-243.wlan.ic.ac.ukr Processing9K O<wjoshuadavies%0 PCf1zero]Q first@N Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321@ Parameterse-  MestReNovaZ macOS 10.16dyn3146-243.wlan.ic.ac.ukManual Peak Picking9K O<wjoshuadavies%0D To@S23rFrom@fJRegion @3I" Threshold19.96000531555336 "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method StandardParamse-  MestReNovaZ macOS 10.16dyn3146-243.wlan.ic.ac.ukManual Peak Picking9K O<wjoshuadavies%0D To@5G&|\From@LnMRRegion @R3/p# Threshold75.175048633505639 "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method StandardParamsd-  MestReNovaZ macOS 10.16dyn3155-59.wlan.ic.ac.ukZoom9K O<wjoshuadavies%I/* [7.04585, 199.025]$ Horizontal[7.04585, 199.025]+ [-47.2205, 434.073]#Vertical[-47.2205, 434.073]d-  MestReNovaZ macOS 10.16dyn3155-59.wlan.ic.ac.ukZoom9K O<wjoshuadavies%ID* [10.1595, 191.019]$ Horizontal[10.1595, 191.019]+ [-47.2205, 434.073]#Vertical[-47.2205, 434.073]e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.local Full Zoom Out9K O<wjoshuadavies%JN + [-31.1545, 251.157]% Horizontal[-31.1545, 251.157]+ [-47.2205, 434.073]#Vertical[-47.2205, 434.073]e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localZoom9K O<wjoshuadavies%Jj+ [-9.85688, 189.951]% Horizontal[-9.85688, 189.951]+ [-47.2205, 434.073]#Vertical[-47.2205, 434.073]e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localIncrease Intensity9K O<wjoshuadavies%Jn+ [-41.7667, 383.939] Scale[-41.7667, 383.939]e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localAutomatic Baseline Correction9K O<wjoshuadavies%Jxy f1 To@oeoiSel Reg AutoRun RegionPoly OrderMulti Point Lambda AutodetectFrom?' 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D2O@Y@Y@Y@Y@Yr b?:26,:?(:>. &֕?6C-@I???@& ?6C-?@@$?@.@.@$ & ?6C-??@Y?d 2D$????zG{8# # # # # # #               h: ! ) ! ) @4@(=# <????zG{??????????bD0$?@Y?zG{h: !  !  @4@( =# <?ٙC@@U???????h: ! z) ! z) @4@( =# =L_!@???ffffff?@V??ffffff?????????333333_!@???ffffff@@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333       l_Z% a\nBa?5Zg% nBa?5Zgk4,l5?5Zg@SCd:a\% _Z% _Z% _Z% _Z%   ?Ee0  !de0 ?'@oeoi !de0  !de0  !de0  !de0  !de0  !d? ? ? ? ? ? ? ?r b?:2ޗB,:?(:>. &֕?6C-@I???@& ?6C-?@$@$?@.@.@$ *@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{#(1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard3}(LVp@@oeD;?' \@eAOҙ@Ch ;?N76"?N76"1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard)F^зE67j 4@oeD;?' \@ac@JCB?6(?6(1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardYf G@Ԅֆ@oeD;?' \@a3 Q)@C[)OCt?P`?P`1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard(HwN'@oeD;?' \@`y]@Bq?K-?K-1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardHϞU~@oeD;?' \@`9ʷ@oD^n???1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standardt@xD!#`˦@oeD;?' \@`!+' `@h?d?d1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard/5tNUA֐@oeD;?' \@` ,@khh0?G?G1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardsVeM'f@oeD;?' \@_l/7@Yt'.?\a?\a1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard\SKՈU @oeD;?' \@]iCl@f)&;w?rzd?rzd1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard7@̑t ȵ@oeD;?' \@SWBl@xM|=dn?Vf?Vf1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standardd̃TJ۞VŷT@oeD;?' \@SCLIH@x̕Cӯ?^g"E?^g"E1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard[VPAP- @oeD;?' \@S2[a@KƠ?-vЖ?-vЖ1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standardsݳz8MVIa@oeD;?' \@C)x@X.??1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standardv;[L΁_~T #u@oeD;?' \@>,B5t@Y#+n\f?? T/Volumes/Av400C/brad/nmr/Jul13-2021/31/fid