Mestrelab Research S.L.B$.AppleSystemUIFont@22{index}?$$.AppleSystemUIFont@22{name, 0}?e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localZDocument Items ParentshipSnθtKM|joshuadavies%e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localZDocument Items ParentshipSnθtKM|joshuadavies%CnMestReNova14.0.0-23239SnθtKM|nbVPW-  MestReNovaZ macOS 10.16 Joshuas-MBPCreate Item (Text)h͍,Bfrjoshuadavies% Text Item TypeTextr Type Report SpecialSubType Peaks,1HMetadataW-  MestReNovaZ macOS 10.16 Joshuas-MBP%Edit text itemh͍,Bfrjoshuadavies%.c  Peak Report

1H NMR (400 MHz, CDCl3) δ 8.41, 7.78, 7.78, 7.76, 7.76, 7.45, 7.45, 7.43, 7.43, 7.42, 7.41, 7.41, 7.41, 7.30, 7.30, 7.28, 7.28, 7.27, 7.27, 7.26, 7.18, 7.16, 6.96, 6.94, 3.92, 2.26.

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 8.41, 7.78, 7.78, 7.76, 7.76, 7.45, 7.45, 7.43, 7.43, 7.42, 7.41, 7.41, 7.41, 7.30, 7.30, 7.28, 7.28, 7.27, 7.27, 7.26, 7.18, 7.16, 6.96, 6.94, 3.92, 2.26.

W-  MestReNovaZ macOS 10.16 Joshuas-MBPMove selectionh͍,Bfrjoshuadavies%0  Text Item TypeText @ x5321 @i y6249W-  MestReNovaZ macOS 10.16 Joshuas-MBP%Edit text itemh͍,Bfrjoshuadavies%F  Peak Report

1H NMR (400 MHz, CDCl3) δ 8.41, 7.78, 7.78, 7.76, 7.76, 7.45, 7.45, 7.43, 7.43, 7.42, 7.41, 7.41, 7.41, 7.30, 7.30, 7.28, 7.28, 7.27, 7.27, 7.26, 7.18, 7.16, 6.96, 6.94, 3.92, 2.26.

Text Peak Report

1H NMR (400 MHz, CDCl3) δ 8.41, 7.78, 7.78, 7.76, 7.76, 7.45, 7.45, 7.43, 7.43, 7.42, 7.41, 7.41, 7.41, 7.30, 7.30, 7.28, 7.28, 7.27, 7.27, 7.26, 7.18, 7.16, 6.96, 6.94, 3.92, 2.26.

e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localDelete Item (Text)h͍,Bfrjoshuadavies% Text Item TypeTextW-  MestReNovaZ macOS 10.16 Joshuas-MBPCreate Item (Text))v`L33ݸ ,joshuadavies%Ζ  Text Item TypeTextt Type Report SpecialSubType Peaks,13CMetadataW-  MestReNovaZ macOS 10.16 Joshuas-MBPMove selection)v`L33ݸ ,joshuadavies%Π4 Text Item TypeText @ x5306 @< y6204W-  MestReNovaZ macOS 10.16 Joshuas-MBPEdit text item)v`L33ݸ ,joshuadavies%ά   Peak Report

13C NMR (101 MHz, CDCl3) δ 173.34, 137.96, 135.66, 131.43, 130.83, 129.49, 128.49, 128.01, 127.72, 126.95, 43.35, 21.16.

Text Peak Report

13C NMR (101 MHz, CDCl3) δ 173.34, 137.96, 135.66, 131.43, 130.83, 129.49, 128.49, 128.01, 127.72, 126.95, 43.35, 21.16.

e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localEdit text item)v`L33ݸ ,joshuadavies%M  Peak Report

13C NMR (101 MHz, CDCl3) δ 173.34, 137.96, 135.66, 131.43, 130.83, 129.49, 128.49, 128.01, 127.72, 126.95, 43.35, 21.16.

Text Peak Report

13C NMR (101 MHz, CDCl3) δ 173.34, 137.96, 135.66, 131.43, 130.83, 129.49, 128.49, 128.01, 127.72, 126.95, 43.35, 21.16.

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T/Volumes/Av400A/brad/nmr/Dec01-2021/10/fidData File Name =brukerExpName(datafile(_FILEPATH_), parm.txt(NAME), parm.txt(EXPNO), parm.txt(PROCNO))"Dec01-2021.10.fid Title *=Str.trimStr(title())jd_348BComment  acqus ORIGIN&Bruker BioSpin GmbH Origin  acqus OWNERnmr Owner Site  acqus$INSTRUM spectInstrument  Author  acqus$SOLVENT CDCl3Solvent  acqus$TE294.2624Temperature  acqus$PULPROGzg30Pulse Sequence L=brukerExperimentType(acqus($PULPROG))1DExperiment  acqus$PROBHDT5 mm PABBO BB/19F-1H/D Z-GRD Z108618/0624 Probe  acqus$NS16Number of Scans  acqus$RG 207.33Receiver Gain  acqus $D[1]1 Relaxation Delay  acqus $P[1] 11.25Pulse Width  =brukerPresatFreq(acqus($PULPROG), acqus($SPOFFS[6]), acqus($SFO1), acqus($O1), acqus($SW), procs($OFFSET), fq0list()) .Presaturation Frequency j=brukerAQ(parm.txt(AQ;;;1), acqus($SW_h), acqus($TD))2.0447233 Acquisition Time v=brukerDate2(acqus($DATE), parm.txt(Date_), parm.txt(Time))&2021-12-01T13:11:00 Acquisition Date  acqus_LASTMODIFIED_&2021-12-01T13:11:43"Modification Date  Class   %100 Purity  0 Spectrum Quality 400.41240246,Spectrometer Frequency  8012.82051282051Spectral Width "-1603.95025642547 Lowest Frequency 1HNucleus .=Utl.div(acqus($TD), 2) 16384Acquired Size  65536Spectral Size  "0.122265938000801 $Digital Resolution $Absolute Reference/ uxnmr.par%ڀ%% X`x\Ys6~&ڵRR(q#J IٞyIic O[!ՙz#_¡mM+OU^;L̍-i5K Ӂeږm[-ocd}W nyfX"x݊\.+ZQzs!DFLy~e¤uq}w d8` c"cpQ-Q8UDԇrl)hafº(M&Zẅ́7Qmϟ_YMJ~N2aJK%J<:O rt@X;Di퐣cCvHRCյJ4u{lh{lzDi(a2>ʵ:0}}=2iK{XڣȮ'B"I Ud"YzE6*rjPJ˘ #iyQH48H&>ZQQ#*r1dQ-ãxǻL֏?UaJTXwWO޾T= YH9/a\.X'Ԡz2(,zĊ>ir+jZnVRJ%eؠTjRkBjMH 7!&ф7! 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e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localw Create PageQO$8djoshuadavies%   At5i(66@'>|@r66 (#QO$8dizirijm[ (@o0JK\T<& e-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localDImport Item (NMR Spectrum)( OM1H)joshuadavies%u$ NMR Spectrum Item Type NMR Spectrum Filename T/Volumes/Av400A/brad/nmr/Dec01-2021/11/fidMetadatae-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localr Processing( OM1H)joshuadavies% PCf1zerocTɅ first@;E Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321@ Parameterse-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localManual Peak Picking( OM1H)joshuadavies%D To3>l(From@f|TngRegion @E`4# Threshold43.823258901305508 "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method StandardParamse-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localAutomatic Baseline Correction( OM1H)joshuadavies%Hy f1 To@nlCSel Reg AutoRun RegionPoly OrderMulti Point Lambda AutodetectFrom4P Filter AutodetectExclude CutsAlgorithm PolyFit Parameterse-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.local.Automatic Phase Correction( OM1H)joshuadavies%J f1 Method AutoAuto Method Start PH1@;EStart PH0cTɅStack PH1Stack PH0$Single Stack PhaseRef Stack SpcInit Mode InitImportedAuto 1D Regions AnalysisApplied Parameterse-  MestReNovaZ macOS 10.16Joshuas-MacBook-Pro.localSet NMR Spectrum Properties( OM1H)joshuadavies%Zsr9 TitleVisible TitleVisible Properties1D13C( OM1H)( OM1H)@@Q?@ NMR SpectrumNMR@@@@Z>@0 u]XP, vD}@j&L2e.SF NS Text@>2MNova Default4,Orange-Cyan (Gradient) UBϐ}CrYM78"|mUUnqǹ*@:8U~NXnJwF^=:?^=1?nJwF?~NTz?@:Q?f(?"|m?YM/?ϐ}C@? 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T/Volumes/Av400A/brad/nmr/Dec01-2021/11/fidData File Name =brukerExpName(datafile(_FILEPATH_), parm.txt(NAME), parm.txt(EXPNO), parm.txt(PROCNO))"Dec01-2021.11.fid Title *=Str.trimStr(title())jd_348BComment  acqus ORIGIN&Bruker BioSpin GmbH Origin  acqus OWNERnmr Owner Site  acqus$INSTRUM spectInstrument  Author  acqus$SOLVENT CDCl3Solvent  acqus$TE295.0771Temperature  acqus$PULPROG zgpg30Pulse Sequence L=brukerExperimentType(acqus($PULPROG))1DExperiment  acqus$PROBHDT5 mm PABBO BB/19F-1H/D Z-GRD Z108618/0624 Probe  acqus$NS480Number of Scans  acqus$RG 207.33Receiver Gain  acqus $D[1]1 Relaxation Delay  acqus $P[1]9.6Pulse Width  =brukerPresatFreq(acqus($PULPROG), acqus($SPOFFS[6]), acqus($SFO1), acqus($O1), acqus($SW), procs($OFFSET), fq0list()) .Presaturation Frequency j=brukerAQ(parm.txt(AQ;;;1), acqus($SW_h), acqus($TD))0.6225920 Acquisition Time v=brukerDate2(acqus($DATE), parm.txt(Date_), parm.txt(Time))&2021-12-01T13:25:00 Acquisition Date  acqus_LASTMODIFIED_&2021-12-01T13:25:25"Modification Date  Class   %100 Purity  0 Spectrum Quality  100.694248477066,Spectrometer Frequency  26315.7894736842Spectral Width "-2084.41767085039 Lowest Frequency 13CNucleus .=Utl.div(acqus($TD), 2) 16384Acquired Size  65536Spectral Size  "0.401547080592105 $Digital Resolution $Absolute Reference2 uxnmr.par%ep%h%( X`x\Ys6~&ڵRR(q#J IٞyIic O[!ՙz#_¡mM+OU^;L̍-i5K Ӂeږm[-ocd}W nyfX"x݊\.+ZQzs!DFLy~e¤uq}w d8` c"cpQ-Q8UDԇrl)hafº(M&Zẅ́7Qmϟ_YMJ~N2aJK%J<:O rt@X;Di퐣cCvHRCյJ4u{lh{lzDi(a2>ʵ:0}}=2iK{XڣȮ'B"I Ud"YzE6*rjPJ˘ #iyQH48H&>ZQQ#*r1dQ-ãxǻL֏?UaJTXwWO޾T= YH9/a\.X'Ԡz2(,zĊ>ir+jZnVRJ%eؠTjRkBjMH 7!&ф7! 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?@?@?d??zG{6,vq[VJ @r@@UnknownCDzd@ (\)@ =p @M@N?tzG{(@YAׄ@9%u*DSS methyl signal D2O@Y@Y@Y@Y@Yr b?:2SP ,:?(:>. &֕?6C-@I???@& ?6C-?@@$?@.@.@$ & ?6C-??@Y?d 2D$????zG{8# # # # # # #               h: ! ) ! ) @4@(=# <????zG{??????????bD0$?@Y?zG{h: !  !  @4@( =# <?ٙC@@U???????h: ! ) ! ) @4@( =# =L_!@???ffffff?@V??ffffff?????????333333_!@???ffffff@@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333_!@???ffffff?@V??ffffff?????????333333       l_Z% a\41?֡u% 41?֡uOOD?֡u@SB Pa\% _Z% _Z% _Z% _Z%   ?Ee0  !de0 4P@nlC !de0  !de0  !de0  !de0  !de0  !d? ? ? ? ? ? ? ?r b?:2ޗB,:?(:>. &֕?6C-@I???@& ?6C-?@$@$?@.@.@$ *@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{*@ @Y?zG{((1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardF٨08B:80f@nlu4т@dqW@O.,??1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardFb-A4F@nlu4т@al@aKW)R?ʆ?u?ʆ?u1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardYnI,Şyj@nlu4т@a+|@M7dD?DW/B?DW/B1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardyE ]2Q@nlu4т@`V6@O.:/R?8?81,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard Ci(#@nlu4т@`cp@Mx9Y?]F[:x?]F[:x1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardE|O&mV2@nlu4т@`71`O@a Y?N)?N)1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardҥfEIww@nlu4т@`.y9Ҝ@n5j?Ƙt?Ƙt1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardMHnEb"L@nlu4т@`ԍ=]0@qjg>?nY?nY1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard7;H>!9@nlu4т@_ot@m%"?Q/F?Q/F1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard(aLn+FjEV@nlu4т@_,g>@pn?Yۉ?Yۉ1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standardq䷤:rE6i4p@nlu4т@^s(<@`LX9?a?a1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardBiÄHcN!=@nlu4т@SWL7@=?׬ƥ?׬ƥ1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard8;Jm' -f@nlu4т@SB%i@r ?w 3?w 31,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standardx_F e?@nlu4т@S.sΩ@DN?E]?E]1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method Standard{RC#LbRK @nlu4т@EFb@a(4u?ݲ?ݲ1,$}uloptions "PP: {Apply: false, Sensitivity: 10, Parabolic: true, Noise Level: 10, PeakType: Positive, MaxPeaks: 1000, MergeMult: false, F2Max: 15, F1Max: 15} method StandardeNDOƩ @nlu4т@5!o@Y 烽?KxA?KxA T/Volumes/Av400A/brad/nmr/Dec01-2021/11/fid